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GCMS scan comments for sample AD31017

Machine-extracted title · confidence 95%

Laboratory note stating that the GCMS scan of sample AD31017 did not reveal unusual compounds on January 18, 2002.

NYC-WTC_000017364–000017379

Folder label: “GCMS X 12/20/01 A 1/8/02

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NYC 9/11 Public Portal Document Library Search Compound Report *. + “pata File : C:\HPCHEM\1\DATA\JAN0802\31017.D Vial: 13 Acq On : 9 Jan 2002 1:02 am Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L JESSIE ISIE IIS ISI IIIS IIOEI ISIS IOI SSIS ISOS UI IO II Peak Number 8 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 9 R.T. EstCone Area Relative to ISTD R.T. 26.73 0.43 ug/l 149083 Phenanthrene-d10 24.81 Hit# of 5 Tentaive ID MW MolForm cas# Qual 1 Trisiloxane, J/1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 42 2 3-Isopropoxy“1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 38 3 Ethanediojé acid, bis(trimethylsily 234 C8H18s04si2 018294-04-7 32 .4_2-Hexengdioic acid, bis(trimethylsi 288 C12H2404Si2 _055494-10-5 32 Abundance ‘Scan 2363 (26.734 min): 31017.D (-) m/z 73.00 100. “ | | | 5000: i 147 zt ae 385 429 26.40_26.60 26,80 27.00 4s als toty | 248) Sa ATS epee) m/z 147.00 33.76 ‘Abundance 6 ae Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet | | (i | | | | 281 AK | 26.40 26.60 _26.80_27.00 | 369 | m/z 281.00 16,508 207 249 398 t miz—> ‘0 100. 150. 200” 250° 300. 360 400450. 600 560 | ‘Abundance | Li i ] 28.40 28.60 28.80 127.00 _ 5000} m/z ae 13.57 | 147 21 281 } 327 415 510561 | | Abundance #30580; Ethanedioic acid, bis(timethyisilyl) ester 7} 147 __ 26.40 28.60 26.80 27.00 m/z 74.00 3.23% 5000 45 | mz> "80100. 190200 250 300 350 400 460 500 580 | 2640 26160 280 a0 | 31017.D GCMSO103.M Wed Jan 09 12:04:00 2002 Page 8 NYC-WTC_000017377

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NYC-WTC_000017377Source: NYC Law Department, mirrored locally

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