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GCMS scan comments for sample AD31017

Machine-extracted title · confidence 95%

Laboratory note stating that the GCMS scan of sample AD31017 did not reveal unusual compounds on January 18, 2002.

NYC-WTC_000017364–000017379

Folder label: “GCMS X 12/20/01 A 1/8/02

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Scanned page image, NYC-WTC_000017378
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NYC 9/11 Public Portal Document Library Search Compound Report *. 4 "pata File : C:\HPCHEM\1\DATA\JAN0802\31017.D Vial: 13 Acq On : 9 Jan 2002 1:02 am Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title + 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Prevrettrrrrrrererrrrrrererrrtrrrttrretririr irre rir i ill tlt l lll Peak Number 9 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 8 R.T. EstCone Area Relative to ISTD R.T. 32.93 0.47 ug/1 106823 Chrysene-d12 32.84 Hit# of 5 Tentative ID MW MolForm caAs# Qual 1 3-Isopropoxy1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 40 2 Ethanediojé acid, bis(trimethylsily 234 Cs8His04si2 018294-04-7 25 3 Mercaptgdcetic acid, bis(trimethyls 236 CeH2002ssi2 006398-62-5 17 4 3-Triméthylsilyloxystearic acid, tr 444 C24H5203Si2__000000-00-0 17 Abundance ‘Scan 3038 (82.931 min): 31017.D () | m/z a “100. 00% | \ | | 5000+ 147 i 21 | os | 281 | Seen te tay {39 497 191 2s) 8 |__‘s2te0 ‘32180 "33.00 33.20 t tre nee m/z 147.00 44.50 mizn>____50 100 150200 __250__300__350___400__450.__500__550. Abundance ra #80503: B-sopropony-1,1,1,7,7,7hexamethyi-3.5,5-trs( tim | i e000 147 "3260 "s2le0 ‘3300 3320", | m/z 220.9 22.59 mr 281 aay me ao oH ig | mz-> 80 100 160 200 250. 300. 360 400 480 600 660, i / ‘Abundance, ’ 5 5 | 2 147 ‘3260.32.80 33.00 3020. +5000: m/z 281.09 16.99 , | 447 {0210 | miz->____50__100__ 150 ___200_ 250 _300___350___400___450_500_550 ‘Abundance #30948: Mercaptoacatic acid, bis(trimethyisilyl)- | Bsa ~‘sdleo_szls0_s3100 5520" | m/z 355.00 16.03% 221 | | mi 104 ue | miz-> "so 100. 150 200 250 300 350 400 450 500 50 92.60 32.80 33.00 33.20 31017.D GCMS0103.M Wed Jan 09 12:04:05 2002 Page 9 NYC-WTC_000017378

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NYC-WTC_000017378Source: NYC Law Department, mirrored locally

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