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GCMS analysis log for sample AD31024

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31024 performed on January 18, 2002.

NYC-WTC_000017494–000017513

Folder label: “GCMS X 12/20/01 A 1/8/02

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Scanned page image, NYC-WTC_000017511
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NYC 9/11 Public Portal Document Library Search Compound Report _ ‘" pata File : C:\HPCHEM\1\DATA\JAN0802\31024.D Vial: 16 Acg On : 9 dan 2002 3:58 am Operator: 209 GALOS Sample : gems scan 12/20 Inst + GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L JESSE SS IHS S IS ISSO SSIS TOSI SIS SIGE ICIS O ISI SSIS ISIS IOI SGI ISTO Peak Number 11 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 11 R.T. EstCone Area Relative to ISTD R.T. 31.56 0.56 ug/l 120350 Chrysene-d12 32.84 Hit# of 5 Tentative ID MW MolForm cAS# Qual 1 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 42 2 Ethanedioic acid, bis(trimethylsily 234 C8H1804si2 018294-04-7 38 3 2-Hexenedioic acid, bis(trimethylsi 288 C12H2404Si2 055494-10-5 23 _4 Butanoic acid, 3-methyl-2-[(trimeth 262 C11H2603Si2 055124-92-0 23 Abundance “Scan 2886 (31.560 min): 31024.D ¢) Tm/z mi 100.00 | 7 2p 355. “3120. saat hs “aie 429 (4031.60. 31. 45 417, 191 ser, [491 We ta 00 aL BS miz> 60100150 200 _250 _300__350_400__450__500_ _550__| | “Abundance #60503: 3-isopropoxy-1,1,1,7,7,7-hexamethyl-3,5, 5-tris(trim: oe | 147 |__31.20 31.40 _31.60_31.80 m/z 221.0 24.05 224 281 327 as 5 + eer be penitent ep BL mvz->__80 100 150 __200 250 _300__350 400 __ 450.500. 550. | [Abundance Teo Gat bistiimeih e | 73 147 31:20 3140 31.60 31.80 5000. m/z 281.00 15.16 | 45 \ Cp eee | te->___50__100 150.200 _250__300___350 __400_450__500_§50_| | Abundance #40777; 2-Hexenedioic acid, bis(trimethylsily!) ester, (E)- r 31.20 31.40 31.60_ 31.80 m/z 355.05 11.73) 5000: | a 147 412 244 273 : mz-> "60 100 150 200 250 300 950 400 450 500 660 | 3120 3140 31.60 3180 | 31024.D GCMS0103.M Wed Jan 09 12:15:30 2002 Page 11 NYC-WTC_000017511 7

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NYC-WTC_000017511Source: NYC Law Department, mirrored locally

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Log entry documenting a gas chromatography-mass spectrometry analysis of unknown compounds in sample AD31020 on January 18, 2002.

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Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31073 performed on January 18, 2002.

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GCMS analysis log for sample AD31076 · Box DEP Box 16

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Log entry documenting a gas chromatography-mass spectrometry analysis of unknown compounds in sample AD31076 on January 18, 2002.

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GCMS blank analysis results · Box DEP Box 16

NYC-WTC_000017344

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