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GCMS analysis log for sample AD31024

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31024 performed on January 18, 2002.

NYC-WTC_000017494–000017513

Folder label: “GCMS X 12/20/01 A 1/8/02

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NYC 9/11 Public Portal Document Library Search Compound Report ‘* * pata File : C:\HPCHEM\1\DATA\JAN0802\31024.D Vial: 16 Acq On : 9 Jan 2002 3:58 am Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L eererrererrrirre restr sterirrrrrtrtrtittriitrt tits tri titi irri rrr ry Peak Number 12 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 9 R.T. EstConce Area Relative to ISTD R.T. 32.93 0.73 ug/l 158349 Chrysene-d12 32.84 Hit# of 5 Tentative ID MW MolForm cas# Qual 1 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 40 2 Ethanedioic acid, bis(trimethylsily 234 CsH1804si2 018294-04-7 32 3 Mercaptosuccinic acid, tris(trimeth 366 C13H3004SSi3 000000-00-0 23 4 2-Hexenedioic acid, bis(trimethylsi 288 C12H2404Si2 _—055494-10-5 23 ‘Roundance ‘Scan 3087 (82.028 min): 31024. ¢) m/z 73.00 100.008 ‘5000 147 | * 281 355 ‘ Boh ed et 325 | tot TE ep m/z 147.00 42.07 Abundance ' #60503: 3-isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 5000. _ 147 00 32.80 33.00 33.20 m/z 221.0, 24.40 mz-> "80 100.150 200. 250 300 380 400 450 500 500 ‘Abundance ; \ a “a7 |___32160 32.80 33.00 33.20 15000 m/z aan 14.33 45 47, 190 219 \ mz—>__ "80.100 480 200" 250 300 960 400450 "500 580 _ | Abundance #50900; Mercaptosuccinic acid, tris(trimethyisilyl) ester 32.60 32.80 33.00 33.20 m/z 281.0 13.64 5000! | 147 245 276 990 951 | | m2—> 0100 150 200 250 300 350 400 460 600 560, 32.60 32.60 33.00 33.20 | 31024.D GCMS0103.M Wed Jan 09 12:15:35 2002 Page 12 NYC-WTC_000017512

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NYC-WTC_000017512Source: NYC Law Department, mirrored locally

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GCMS scan comments for sample AD31017 · Box DEP Box 16

NYC-WTC_000017364

Laboratory note stating that the GCMS scan of sample AD31017 did not reveal unusual compounds on January 18, 2002.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998

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GCMS analysis log for sample AD31020 · Box DEP Box 16

NYC-WTC_000017459

Log entry documenting a gas chromatography-mass spectrometry analysis of unknown compounds in sample AD31020 on January 18, 2002.

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GCMS analysis log for sample AD31073 · Box DEP Box 16

NYC-WTC_000017434

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31073 performed on January 18, 2002.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996

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GCMS scan comments for sample AD30605 · Box DEP Box 16

NYC-WTC_000017265

Laboratory note stating that the GCMS scan of sample AD30605 did not reveal unusual compounds on January 22, 2002.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996

machine-extracted · confidence unavailable · Check page ↗
GCMS analysis log for sample AD31076 · Box DEP Box 16

NYC-WTC_000017514

Log entry documenting a gas chromatography-mass spectrometry analysis of unknown compounds in sample AD31076 on January 18, 2002.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996

machine-extracted · confidence unavailable · Check page ↗
GCMS blank analysis results · Box DEP Box 16

NYC-WTC_000017344

Laboratory report listing detection limits for numerous organic compounds in a GCMS blank sample analyzed on January 10, 2002.

1 shared topics · Same agency, volume and box · similarity 0.994

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