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GCMS scan comments for sample AD31017

Machine-extracted title · confidence 95%

Laboratory note stating that the GCMS scan of sample AD31017 did not reveal unusual compounds on January 18, 2002.

NYC-WTC_000017364–000017379

Folder label: “GCMS X 12/20/01 A 1/8/02

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Scanned page image, NYC-WTC_000017376
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NYC 9/11 Public Portal Document Library Search Compound Report “)* Data File : C:\HPCHEM\1\DATA\JAN0802\31017.D Vial: 13 Acq On : 9 Jan 2002 1:02 am Operator: 209 GALOS Sample + gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L eeverwrerrrrr Tr rer rere rerrrrrrrrrrrtrrirrr itt rittt titi titer rrr ttt t ry Peak Number 7 N-(Trifluoroacetyl)-0,0',O''-t Concentration Rank 6 R.T. | EstCone Area Relative to ISTD R.T. 22.64 1.11 ug/1 379947 Phenanthrene-d10 24.81 Hit# of 5 Tentative ID MW MolForm cas# Qual 1 N-(Trifluoroacgtyl) -0,0',0''-tris(t 481 C19H34F3NO4Si3 000000-00-0 35 2 Benzeneethangfiine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 35 3 Benzoic acj@, 2,5-bis(trimethylsilo 370 C16H3004Si3 003618-20-0 25 4 N-(Triflyéroacetyl) -N,0,0',0''-tetr 553 C22H42F3NO4Si4 000000-00-0 22 Abundance ~~ Sean 1917 (22,640 min): 31017.D ©) m/z =e 100.008 7 — VO nD 401 2240 22.60 22.80 23.00 48 27 __, 2240_22.860_ 2: x Wag Ma PL oom) The 7-99 26.94" miz-> 90.400. 180__200__250__300__ 350__400__450_500__ 550 _ ‘Abundance #58326: N-(Trifidoroadsiyi)-O,07/0"-tris(iimethyally}jno i rc} 356 5000 ’ 22.40 22.60 22.80 23.00 is | m/z 385.95 25.50% 4 120147 193 265, i 481 } mz-> 60 100 150° 200° 250° 300° 350° 400450. 600 580 | ‘Abundance 8 355, 2240 22.60 2280 23100 ‘5000: m/z 221.0 19.84 be , 208 _251 281 386458 548__| Perper pe oer eee ren a re miz->____50___100 150 _200 250 300 350 400 450___ 500.550 Abundance: #73978: Benzoic acid, 2,5-bis(trimethyisiloxy), trimethyls 1 22.40 22.60 22.80 23.00 | 355 m/z 281.10 14.87% 5000. | 45 | 147 479 223.267 297 7 miz> 30 100 180 200 250° 300 360 400 450.500 "30 “"palao’ 22.60 22180 23100 | 31017.D GCMS0103.M Wed Jan 09 12:03:56 2002 Page 7 NYC-WTC_000017376

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NYC-WTC_000017376Source: NYC Law Department, mirrored locally

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