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GCMS analysis log for sample AD31076

Machine-extracted title · confidence 95%

Log entry documenting a gas chromatography-mass spectrometry analysis of unknown compounds in sample AD31076 on January 18, 2002.

NYC-WTC_000017514–000017528

Folder label: “GCMS X 12/20/01 A 1/8/02

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Scanned page image, NYC-WTC_000017527
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NYC 9/11 Public Portal Document ey Library Search Compound Report " Data File : C:\HPCHEM\1\DATA\JAN0802\31076.D Vial: 9 i Acq On : 8 Jan 2002 9:09 pm Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.1L Peeeeerrerrrrrrerertertrt rrr ret rretr titi ttt rit t itt t cert rt tt tt rrr t ter) Peak Number 7 N-(Trifluoroacetyl)-0,0',O0''-t Concentration Rank 6 R.T. | EstCone Area Relative to ISTD R.T. 22.64 0.42 ug/l 120840 Phenanthrene-d10 24.80 Hit# of 5 Tentative ID MW MolForm cAS# Qual 1 N-(Trifluoroagefyl) -0,0',0''-tris(t 481 C19H34F3NO4Si3 000000-00-0 43 2 Benzoic acid/ 2,5-bis(trimethylsilo 370 C16H30048i3 003618-20-0 43 3 N-(Triflyefacetyl) -0,0',O"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 43 _4 Cycloperftasiloxane, decamethyl- 370 C1OH3005Si5 __000541-02-6 37 ‘Abundance ‘Scan 1916 (22.636 min}: 31076.D (-) [m/z 73.00 100.008 ‘5000 | Ww 224 355 . + 21 45 4 401 22.40 _22.60_22.80_23.00__ — Toe BEE Phen bene m/z 147.00 24.83 mizx>__" "80." 300180200250. 300 950.400 __ 460.500 1 1 ‘Abundance 58526: N{Tritucroacetyl}O,0.O"-is(timethiysilyijno | | 7 | 355 | ® m/z aes OP 20.97% 126147 __ 193 265 a6. 481 | mz—> 50, 100, 150, 200 (250 300. 350 400 450 500 | | ‘Abundance | ] 78 ] 22.40 22.60 22.80 23.00 000] m/z 221.05 15.13 147 479 223267 p07 mz ____50___100 150 __200__250__300__350__400__450__ 500 Abundance #58807: N-(Trifluoracety!)-O,0',0"-tris(trimethyisily/jepin ] + +} 22.40 22.60 22.80 23.00 355, m/z 281.0, 11.64 | 140 104 281 400 | mz> 60 100” 180-200 250 90 350400400. oh0 22.40 22.60 22.80 23.00 31076.D GCMS0103.M Wed Jan 09 12:30:32 2002 Page 7 n NYC-WTC_000017527

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NYC-WTC_000017527Source: NYC Law Department, mirrored locally

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Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31024 performed on January 18, 2002.

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GCMS scan comments for sample AD31017 · Box DEP Box 16

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Laboratory note stating that the GCMS scan of sample AD31017 did not reveal unusual compounds on January 18, 2002.

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GCMS scan comments for sample AD30605 · Box DEP Box 16

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