Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
NYC-WTC_000004149–000004492Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2 701\30710.D Vial: 48 Acq On : 30 Dec 2001 5:23 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 7
R.T. EstConc Area Relative to ISTD R.T.
26.89 0.45 ug/1 257627 Phenanthrene-dl0 24.98
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Trisiloxane,/1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 42 2 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 36 3 Ethanedioid acid, bis (trimethylsily 234 C8H18O4Si2 018294-04-7 32 4 3-1sopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 25 Abundance Scan 2380 (26.892 min): 30710.D (-) m/z 73.00 100.00% 73
5000 147 221 281 26.60 26.80 27.00 27.20 i 45 96 117 • i % 1 — — 1911 [ 249 [ 327325 401.429 m/z 147.00 3 5.32% m/z-> 50 100 150 200 250 300 350 400 450 Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147
281 5000 26.60 26.80 27.00 27.20 369 m/z 281.00 18.09% , 207 249 , 338 . 1 i 4— ----- i m/z-> 50 100 150 200 250 300 350 400 450 (Abundance 858871; 1-Monolingleoyiglycerol trimethylsilyi ether 73
207 26.60 26.80 27.00 27.20 5000 147 m/z 221.05 15.79% 34 103 281 ......395.. 482 m/z-> 50 100 150 200 250 300 350 400 450____ Abundance #30580: Ethanedioic acid, bis(trimethylsilyl) ester i 73 147 26.60 26.80 27.00 27.20 m/z 74.00 8.85% 5000 45 i 110 219 . ....... m/z-> — 504 P 100 150 200 250 300 350 400 450 T IT T 26.60 26.80 27.00 27.20
30710.D GCMS1126.M Mon Jan 28 11:36:38 2002 Page 8
NYC-WTC_000004293
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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
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NYC-WTC_000004148
Fragmented OCR text showing dates and identifiers for a DEP GCMS record dated February 2002.
Filed in the same folder
NYC-WTC_000036712
GCMS analysis report for sample AD29563 listing unknown compounds and surrogate recovery data from January 28, 2002.
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