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Document / 344 pages

DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004149–000004492

Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02”

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Scanned page image, NYC-WTC_000004292
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2 701\30710.D Vial: 48 Acq On : 30 Dec 2001 5:23 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ******************************************************************** * Peak Number 7 Benzeneethanamine, N-[(pentafl Concentration Rank 5

R.T. EstCone Area Relative to ISTD R.T.

22.79 1.18 ug/1 678224 Phenanthrene-dl0 24.98

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 43 2 N-(Trifluor/cetyl)-0,0',0"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 43 3 N-(Trifluoroacetyl)-0,0',0''-tris(t 481 C19H34F3NO4Si3 000000-00-0 37 4 N-(Triflucroacetyl)-N,O,O',O''-tetr 553 C22H42F3NO4Si4 000000-00-0 27 Abundance Scan 1933 (22,788 min): 30710.D (-) m/z 73.00 1 00.00% 73

5000 147 355 221 281 45 401 22.40 22.60 22.80 23.00 23.20 m/z-> — 50 117. 1914 1"rr 249 . ( 327 1 T .L. i" ' ' ' i 1 1 m/z 147.00 25.42% 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene] 73 355

5000 22.40 22.60 22.80 23.00 23.20 45 m/z 355.0 23.62% , J , Il... 208 251 281 386 458 548 miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58807; N-(Trifluoracetyl)-O,O‘.O"-tris(trimethylsilyl)epin 73 355 22.40 22.60 22.80 23.00 23.20 5000- m/z 221.05 16.56%

45 140 184 281 | ______ 480_______ m/z-> 50__ 100 150 200 250 300 350 400 450 500 __ 550 Abundance i 73 #58326: N-(Trifluoroacetyl)-O,O’,O"-tris(trimethylsilyl)no * i ' ■ ,12,... . 22.40 22.60 22.80 23.00 23.20 355 m/z 281.00 12.84% 5000

45 |I 120147 193 265 1 481 ' ‘I ' ’ ' ' ' i ' . ' 1 i ' ' m/z-> 50 100 150 200 250 300 350 400 450 500 550 22.40 22.60 22.80 23.00 23.20

30710.D GCMS1126.M Mon Jan 28 11:36:33 2002 Page 7

NYC-WTC_000004292

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NYC-WTC_000004292Source: NYC Law Department, mirrored locally

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