GCMS analysis results for sample AD30251, Jan 2002

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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30251 conducted on January 9, 2002.

NYC-WTC_000017675–000017691

Folder label: “GCMS X 12/13/01 A 12/27/01”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC2701\30251.D Vial: 8 Acq On : 27 Dec 2001 6:58 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Benzeneethanamine, N-[(pentafl Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 22.79 0.85 ug/1 339429 Phenanthrene-dl0 24.98 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Benzeneethanamine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 25 2 Phenethylamine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 25 3 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 25 4 Benzoic acid, 2,6-bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 20 Abundance Scan 1933 (22.791 min): 30251 D (-) m/ z 73.00 1 00.00% 73

5000 147 355 221 281 401 22.40 22.60 22.80 23.00 23.20 : , 45’ I J 191,, [ 249, I 327 1 . m/z 355.05 27.96% m/z-> 50 100 150 200 250 300 ' ' 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene] 73 355 ........... ........... 5000 22.40 22.60 22.80 23.00 23.20 m/z 147.00 27.63% 45 ' | 208 251 281 386 458 548 11PTITETPTTT I 1 ■ ■ • i ■ ■ ' ■ i ■ ' ‘ ■ i ‘ ■ 111* miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74233 Phenethylamine, N-methy!-.beta.,3.4-tris(trimethyls 73 22.40 22.60 22.80 23.00 23.20 5000 355 m/z 221.05 19.41% 44 147 193 267294 m/z-> ’50 100 150 200 250 300 350 400 450 500 550 ’ Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147 22.40 22.60 22.80 23.00 23.20 281 m/z 281.00 15.14% 5000

369 207 249. I................................. । ! ■ ■ i ' ■ ‘ • i ■ ■ —-PP4 300 ‘ 338 miz-> 50 100 150 200 250 ' 350 400 ' ' 450 ‘ 500 ' 550 2240 22.60 22.80 23.00 23.20

30251.D GCMS1126.M Wed Jan 02 10:38:44 2002 Page 6

NYC-WTC_000017687

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NYC-WTC_000017687Source: NYC Law Department, mirrored locally

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