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Document / 344 pages

DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004149–000004492

Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02

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Scanned page image, NYC-WTC_000004378
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30650.D Vial: 46 Acq On : 30 Dec 2001 3:26 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Benzeneethanamine, N-[ (pentafl Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

22.79 2.96 ug/1 1867940 Phenanthrene-dl0 24.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzeneethanamine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 25 2 N-(Trifluoroacetyl) -N,O,O1,O'1-tetr 553 C22H42F3NO4Si4 000000-00-0 22 3 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 20 4 Benzoicacid, 2,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 17 Abundance Scan 1933 (22.791 min): 30650.D (-) m/z 73.00 100.00% 73

5000 147 355 221 281 1 . 22.40 22.60 22.80 23.00 23.20 45 1 11 4 1 117. 191, ..249.1327 1.401 441 m/z 355.05 27.69% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene] 73 355

5000 22.40 22.60 22.80 23.00 23.20 45 m/z 147.00 27.31% 208 251 281 386 458 548 ' ■ i 1 ' m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #01 52: N-/Triflucroacetyh-N,0.0,0-tetrakis(trmethyist 73

355 22.40 22.60 22.80 23.00 23.20 5000 m/z 221.05 19.13%

45 147 193 267 538 m/z--> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethyI-3,5,5-tris(trim 73 22.40 22.60 22.80 23.00 23.20 m/z 281.00 14.77% 5000 147

m/z-> . .. ...271..21, ,3u. . ,59 50 100 150 200 250 300 350 400 450 500 561 550 22.40 22.60 22.80 23.00 23.20

30650.D GCMS1126.M Mon Jan 28 11:18:34 2002 Page 8

NYC-WTC_000004378

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NYC-WTC_000004378Source: NYC Law Department, mirrored locally

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