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← Document results/DEP Box 16/GCMS X 12/18/01 A 12/30/01
Document / 27 pages

GC/MS calibration data for sample 28322, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.

NYC-WTC_000018492–000018518

Folder label: “GCMS X 12/18/01 A 12/30/01

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Scanned page image, NYC-WTC_000018507
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC2701\28322.D Vial: 62 Acq On : 30 Dec 2001 7:56 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Benzeneethanamine, N-[(pentafl Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 22.79 5.74 ug/1 3466900 Phenanthrene-dl0 24.98

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 35 2 N-(Trifluoracetyl)-0,0',0"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 22 3 Benzoic acid, 2,6-bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 20 4 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 20 Abundance Scan 1933 (22.790 min): 28322.D (-) m/z 73.00 100.00% 73

5000 147 355 221 281 22.40 22.60 22.80 23.00 23.20 45 Pr4., 191, -.249.1., 327 — 117 327 4tnii * 1111: 421441 m/z 355.05 28.56% m/z-> 50 100 150 200 250 300 350 400 450 .500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methyiene] 73 355

5000 ■ i ■ ■ ■ ■ i • ‘ ' ‘ 1 1 1 ‘ ‘ I' ' 22.40 22.60 22.80 23.00 23.20 45 m/z 146.95 27.67% 208 251 281 386 458 548 ■ 1 i ■ • FImmi i i । i i i r । > i i > f i1 > । i i ■ i । r ■ i ■ ■ ■ ‘ i ' ■ ■ • i ■ ■ ■ ■ i ■ ■ m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58807; N-(Triluoracety)-Q Mrsftrrel siojt pr 73 355 22.40 22.60 22.80 23.00 23.20 5000 m/z 221.05 19.73%

45 140 184 281 480 ■ ' i • • • ■ i 1 ■ ■ ■ i ■ ■ ■ ' i ' • ' ' i ■ i ' ■ ■ ■ i ■ ' ' ■ i ■ ■ ■ ■ i ‘ miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51296: Benzoic acid, 2,6-bis[(trimethylsilyl)oxy]-, trimet 73 355 22.40 22.60 22.80 23.00 23.20 m/z 281.00 14.89% 5000

147 267 , 47, .... /,1 . +208.41 TIm miz-> 50 100 150 200 250 300 350 400 450 500 550 22.40 22.60 22.80 23.00 23.20 J

28322.D GCMS1126.M Wed Feb 06 12:56:23 2002 Page 10

NYC-WTC_000018507

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NYC-WTC_000018507Source: NYC Law Department, mirrored locally

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