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Document / 27 pages

GC/MS calibration data for sample 28322, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.

NYC-WTC_000018492–000018518

Folder label: “GCMS X 12/18/01 A 12/30/01

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\28322.D Vial: 62 Acq On : 30 Dec 2001 7:56 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 1-Monolinoleoylglycerol trimet Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

26.88 2.92 ug/1 1761640 Phenanthrene-dl0 24.98

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Monolinoleoylglycerol trimethylsi 498 C27H5404S12 054284-45-6 36 2 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 36 3 Ethanedioic acid, bis (trimethylsily 234 C8H18O4Si2 018294-04-7 32 4 2-Pentenoic acid, 2-[(trimethylsily 260 CllH24O3Si2 055045-17-5 23 Abundance Scan 2379 (26.885 min): 28322.D (-) m/ z 72.95 100.00% 73

5000 147 221 281 45 117 1911 249 [ 327.355 401 429 26:60 26.80 27.00 27.20 — ' i ■ ;Pi* i । । f p Pat j 14 Fi" i iS । ri f i^i Pi , । i i । । ■ । i ■ । । । m/z 147.00 31.54% m/z-> 50 100 150 200 250 300 350 400_ 450 500 550 Abundance #58871: 1-Monolinoleoyiglycerol trimethylsily ether 73

5000 147 207 .. n... ’*I’’ * I T * 1T83 J J I J J 1 I 26,60 26.80 27.00 27.20 34 103 281 m/z 281.00 16.43% 395 I 482 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance *60603 s-isepropayya i 1.17.7hxamety.3 5; (-tr 73

26.60 26.80 27.00 27.20 5000 m/z 221.0 15.47% 147 221 281 327 415 l i 519 561 ' ‘ I ' ' ■ ‘ I ‘ ‘ ‘ I ' ‘ ‘ 1 1 1 ‘ ‘ I ' ' ' ‘ I ' ' ' 1 I ‘ ‘ 1 ' 1 ‘ ‘ I ■ ' ‘ ' I ‘' I ' ‘ m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #30580: Ethanedioic add. bis(trimethylsilyl) ester 73 147 26.60 26.80 27.00 27.20 m/z 74.00 8.47% 5000 45

—l TII— 190 219 .... m/z-> 50 100 150 200 250 300 350 400 450 500 550 26.60 26.80 ‘27'00 27.20

28322.D GCMS1126.M Wed Feb 06 12:56:28 2002 Page 11

NYC-WTC_000018508

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NYC-WTC_000018508Source: NYC Law Department, mirrored locally

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