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Document / 344 pages

DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004149–000004492

Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02

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Scanned page image, NYC-WTC_000004349
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC2701\30708.D Vial: 49 Acq On : 30 Dec 2001 6:21 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 1-Monolinoleoylglycerol trimet Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

26.89 1.33 ug/1 867757 Phenanthrene-dl0 24.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Monolinoleoyl^lycerol trimethylsi 498 C27H5404Si2 054284-45-6 36 2 Trisiloxane, /1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 36 3 Ethanedioic id, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 32 4 1,1,1,3,5,5, 7,7-Nonamethyl-3-(tri 384 C12H3604Si5 038146-99-5 28 Abundance Scan 2379 (26.886 min): 30708.D (-) m/z 73.0,0 100.00% 73

5000 147 221 281 45 26.60 26.80 27.00 27.20

m/z-> I T 96 117 1* Hi4., 1911 L . 249, 1 . 327,355. . 401-42% m/z 146.95 33.06% 50 100 150 200 250 300 350 400 450 Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73

207 5000 147 26.60 26.80 27.00 27.20 34 103 m/z 281.00 17.61%

m/z-> 50 100 1,.1*. .395, 150 200 250 300 350 400 1‘I** 450 482

Abundance #74103: Trisiloxane, 1,1,1,5.5,5-hexamethyl-3,3-bisg(trimet 73 147 26.60 26.80 27.00 27.20 5000 m/z 221.05 15.25% 281 45 369 117 ■... 207 249........ i ‘ ‘I m/z-> 50 100 150 200 250 300 350 400___ 450. Abundance #30580: Ethanedioic acid, bis(trimethylsilyl) ester 7|3 147 26.60 26.80 27.00 27.20 m/z 74.00 8.52% 5000 45

i [18 ‘ ' ,I 190 219......... m/z-> 50 100 150 200 250 300 350 400 450 26.60 26.80 27.00 27.20

30708.D GCMS1126.M Mon Jan 28 11:28:59 2002 Page 10

NYC-WTC_000004349

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NYC-WTC_000004349Source: NYC Law Department, mirrored locally

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