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Document / 344 pages

DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004149–000004492

Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02

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Scanned page image, NYC-WTC_000004348
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2 701\30708.D Vial: 49 Acq On : 30 Dec 2001 6:21 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Benzeneethanamine, N-[(pentafl Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

22.79 2.65 ug/1 1726830 Phenanthrene-dl0 24.99 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 37 2 N- (Trifluoracety) -0, 01,0"-tris (tri 495 C20H36F3NO4Si3 000000-00-0 37 3 N-(Trifluoroacettyl)-N,O,O',0''-tetr 553 C22H42F3NO4Si4 000000-00-0 35 4 N-(Trifluoroacetyl)-0,0'z0'1-tris(t 481 C19H34F3NO4Si3 000000-00-0 35 Abundance Scan 1933 (22.792 min): 30708.D (-) m/z 73.00 100.00% 73

5000 147 355 221 281 22.40 22.60 22.80 23.00 23.20 —th504 1 100117. 150 191, 45 j , 249 l 327 [ 401 1 ,.9 443 m/z 355.05 27.88% m/z--> 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyi)methylene] 73 355

5000 22.40 22.60 22.80 23.00 23.20 45 m/z 147.00 27.56% 208 251 281 386 458 548 ■ ' i ‘ ' m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance 458807. N-(Triflugracetyb)-0,0.0"-tris(trimethylsilyl)epin 73 |....... ,.......... 355 22.40 22.60 22.80 23.00 23.20 5000 m/z 221.05 18.90%

45 140 184281; 480 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60162: N-(TrifIuoroacetyl)-N,O,O',O',-tetrakis(trimethyisi ...................................................... 73 22.40 22.60 22.80 23.00 23.20 m/z 281.00 14.70% 355 5000-

45 I ,..... 147 193 267 ..... 1............. 538 ' ‘I 1 • m/z—> 50 100 150 200 250 300 350 400 450 500 550 22.40 22.60 22.80 23.00 23.20

30708.D GCMS1126.M Mon Jan 28 11:28:55 2002 Page 9

NYC-WTC_000004348

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NYC-WTC_000004348Source: NYC Law Department, mirrored locally

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