Laboratory report documenting GCMS analysis for unknown compounds and surrogate recovery in sample AD28335 conducted on January 9, 2002.
NYC-WTC_000033974–000034002Folder label: “GCMS X 11/20/01 A 11/26/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\JAN0 802\28355A.D Vial: 4 Acq On 8 Jan 2002 6:13 pm Operator: 209 GALOS Sample Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 Benzeneethanamine, N-[(pentafl Concentration Rank II
R.T. EstConc Area Relative to ISTD R.T.
28.50 4.92 ug/1 2950560 Phenanthrene-dl0 24.81
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Benzeneethanamine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 25 2 N-(Trifluoroacetyl)-0,0',O' 1-tris(t 481 C19H34F3NO4Si3 000000-00-0 25 3 3-Isopropoxy/1, 1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 23 4 N-(Trifluoracetyl)-O, 01,0"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 17 Abundance Scan 2555 (28.497 min): 28355A.D (-) m/z 73.00 100.00% 73
5000 147 221 355 ) 281 l 28.20 28.40 28.60 28.80 0145 117 V 1+. r I r * r i r 249, .327' —1— 1914— 401 429 . ——... ,... r m/z 147.00 35.95% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-Kpentafluoropheny!)methylene] 73 355
5000 1 28.20 28.40 28.60 28.80 45 m/z 221.05 20.59% L "I 208 251 281 .386 458 548 TTPTTTTT TTuuuumTTTT miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58326. N-(Trifluproacety)-0.O‘,O"-tris(trimethylsilyljno 73 j k TIInnTTTTTTTTT 355 28.20 28.40 28.60 28.80 5000 m/z 355.05 20.12%
45 120147 193 265 TTTTDTTTOTCTRVTUTT 481 TTPPTTTTTTTTTT m/z-> 50 _ 100__ 150 200 250 300 350 400 450 500 550 Abundance #60503:3-lsopropoxy-1,1,1,7,7.7-hexamethyl-3,5t5-tris(trim 73 28.20 28.40 28.60 28.80 m/z 281.00 15.72% 5000 147
221 281 327 • -415 519 561 1 —1— — — — । ' — 1 t ' r T. ’. '. I..'. '..'. '. I’ Trr TT TT m/z-> 50 100 150 200 250 300 350 400 450 500 550 28.20 28.40 28.60 28.30
28355A.D GCMS1126.M Wed Jan 09 09:09:58 2002 Page 13
NYC-WTC_000033994
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NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018287
Analytical notes regarding GCMS scan results and LCS standard recoveries for sample AD30986.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036614
Laboratory comments on GCMS scan results for sample AD29466 noting low recovery and scheduling re-extraction.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018492
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018519
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018470
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000033704
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000033705
Fragmented page from a GCMS-related record dated between November 20 and 26, 2001, likely part of the WTC environmental monitoring series.
Filed in the same folder
NYC-WTC_000033707
Laboratory report of a GCMS blank analysis for sample AD28143 conducted on November 28, 2001, listing various organic compounds below detection limits.
Filed in the same folder
NYC-WTC_000033723
Calibration record for GCMS instrument 209 using method GCMS1126, dated November 26-28, 2001, listing standard compounds and retention times.
Filed in the same folder
NYC-WTC_000033726
Laboratory report of a GCMS reference analysis for sample AD28143 conducted on November 28, 2001, listing detected compounds and retention times.
Filed in the same folder