Analytical notes regarding GCMS scan results and LCS standard recoveries for sample AD30986.
NYC-WTC_000018287–000018315Folder label: “GCMS X 12/27/01 A 1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\JANI802\30986A.D Vial: 3 Acq On 18 Jan 2002 5:36 pm Operator: 209 GALOS Sample Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 Benzeneethanamine, N-[(pentafl Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
22.61 2.70 ug/1 1440780 Phenanthrene-dl0 24.78
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 43 2 N- (Trifluoroacetyl)-N,O,O',0'1-tetr 553 C22H42F3NO4Si4 000000-00-0 43 3 N-(Trifluoracetyl)-0,0’,0«-tris(tri 495 C20H36F3NO4Si3 000000-00-0 37 4 Trisiloxane. 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 37 Abundance. / Scan 1913 (22.608 min): 30986A.D (-) m/ z 72.9.5 100.00% 73
5000 147 355 221 281 22.20 22.40 22.60 22.80 23.00 : 1 454 J 1* i 117 irri191,....................................................... -.249- k , 327 4411m m/z 147.00 26.64% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-K(pentafluoropheny!)methylene] 73 355
5000 22.20 22.40 22.60 22.80 23.00 45 m/z 355.05 25.21% 208 251 281 . 386 458 548 -I—PPT 102/——/— miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60162: N-(Trifluoroacetyl)-N,0,0,0"-tetrakis(trimethylsi 73 .... ....... .........
355 22.20 22.40 22.60 22.80 23.00 5000 m/z 221.05 17.88%
45 : ■ ■ • i ■ ‘ I ‘ i ■ 147 193 . ■ ■ 267 ........ J.......................... 538 m/z- 50 100 150 200 250 300 350 400 450 500 550 Abundance #58807: N-(Trifluoracetyl)-O.O',O"-tris(trimetfiyIsHyl)epin 73 22.20 22.40 22.60 22.80 23.00 355 m/z 281.00 14.10% 5000
45 | 'I 140 184 281 480 ......... I* ‘ ' 1 * 1 ‘ ■ ■ **I****I‘‘SI‘‘*I‘‘SI‘**‘I* IET11//IG—TTTI5SI/18.T m/z~> 50 100 150 200 250 300 350 400 450 500 550 22.20 22.40 22.60 22.80 23.00
30986A.D GCMS1126.M Tue Jan 22 10:18:17 2002 Page 12
NYC-WTC_000018306
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NYC-WTC_000018492
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018519
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018470
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033974
Laboratory report documenting GCMS analysis for unknown compounds and surrogate recovery in sample AD28335 conducted on January 9, 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036614
Laboratory comments on GCMS scan results for sample AD29466 noting low recovery and scheduling re-extraction.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.996
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NYC-WTC_000018058
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NYC-WTC_000018059
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NYC-WTC_000018064
Reference data table listing response factors and concentrations for organic compounds used in GCMS analysis of sample AD30694.
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NYC-WTC_000018069
Blank analysis report showing non-detectable levels of target organic compounds in sample AD30694.
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