Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
NYC-WTC_000019130–000019152Folder label: “GCMS X 12/13/01 A 12/22/01 AND 12/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2701\30256.D Vial: 17 Acq On : 29 Dec 2001 2:47 pm Operator: 209 GALOS Sample : GC/MS SCAN Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Benzeneethanamine, N-[(pentafl Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T.
22.79 3.04 ug/1 1218560 Phenanthrene-dl0 24.99 Hit# of 5 Tentative ID MW MolForm CAS# Qual l Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 35 2 Benzoic acid, /,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 25 3 N-(Trifluoroapetyl)-N,O,O',O1'-tetr 553 C22H42F3NO4S14 000000-00-0 22 4 N-(Trifluoracetyl) 0,0’,0"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 22 Abundance Scan 1933 (22.792 mln): 30256.D (-) m/z 73.00 1 00.00% 73
5000 147 355 221 281 22.40 22.60 22.80 23.00 23.20 45 327 401 0+ I » * j • . . . 191, -.249 ... 4r B*** ■ ' I ‘ 1 ■ • i ■ ■ ■ ' i ' ■ 117 i m/z 355.05 27.89% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene] 73 355 i-111111 — 111111111 5000 22.40 22.60 22.80 23.00 23.20 m/z 147.00 26.44% 45 I 208 251,281 , 386 458 548 ’,1****1*’’14’+I’4’4I***’1+’’’I 10—mBummOTnT ■ ' i I ‘ miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #73978: Benzoic acid. 2.5-bis(trimettylsilaxy)- trimethyls 73 355 22.40 22.60 22.80 23.00 23.20 5000 m/z 221.05 19.30% 45 j 147 179 223 267297 j m/z-> 50 100 150 200 250 300 350 400 450 500 550 ... 4..... Abundance #60162: N-(Trffluoroacetyl)-N,O,O',O"-tetraWs(trimethylsi 73 22.40 22.60 22.80 23.00 23.20 rn/z 281.00 14.86% 355 5000
45 147 193 267 538 • • i ’ 11 1 1 1 ' '1 I 11' r i ' ' 1 ' 1 1 *f*******1*441****|*V*/* m/z-> 50 100 150 200 250 300 350 400 450 500 550 22.40 22.60 22.80 23.00 23.20
30256.D GCMS1126.M Wed Jan 02 10:24:44 2002 Page 8
NYC-WTC_000019144
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NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017833
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017724
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30426 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017808
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30352 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017675
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30251 conducted on January 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036712
GCMS analysis report for sample AD29563 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036798
GCMS analysis report for sample AD29523 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000019035
Fragment of a GCMS document collection from December 2001 with minimal visible text.
Filed in the same folder
NYC-WTC_000019036
Record of Method 502 GCMS analysis data and quality control parameters for samples analyzed in December 2001.
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NYC-WTC_000019040
Calibration report for gas chromatography-mass spectrometry analysis of nitrosamines and chlorinated benzenes conducted on December 22, 2001.
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NYC-WTC_000019044
Reference analysis report for gas chromatography-mass spectrometry quantification of volatile organic compounds conducted on December 29, 2001.
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NYC-WTC_000019049
Laboratory report documenting gas chromatography-mass spectrometry blank analysis for volatile organic compounds conducted on January 7, 2002.
Filed in the same folder