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GC/MS calibration data for sample 28323, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.

NYC-WTC_000018519–000018545

Folder label: “GCMS X 12/18/01 A 12/30/01

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Scanned page image, NYC-WTC_000018535
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC2701\28323.D Vial: 63 Acq On : 30 Dec 2001 8:55 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 1-Monolinoleoylglycerol trimet Concentration Rank II

R.T. EstConc Area Relative to ISTD R.T.

26.89 4.33 ug/1 3063220 Phenanthrene-dl0 24.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 36 2 Trisiloxane,/!,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 36 3 1,1,1,5,7, <7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 35 4 3-Isopropq y-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 34 Abundance .... ) Scan 2379 (26.888 min): 28323.D (-) m/ z 73.00 100.00% 73

5000 147 221 281 ■ • 1 i • ■ ■ ■ i r ■ ■ ■ i 1 ■ ‘ 1 i • • ■ ‘

45 , 191 l [ 249 . [ 327 325 401 429 26.60 26.80 27.00 27.20 96 117,, , TIr ।-i j' i i F1“ । T*I—nETTTETBTETT m/z 147.00 33.32% miz-> 50 100 150 200 250 300 350 400 450 Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether 73

207 5000 147 ■ Kmndamndmm/m/nn 26.60 26.80 27.00 27.20 34 103 1 281 m/z 281.00 18.18% | 395 482 m/z-> 50 100 150 200 250 300 350 400 450 Abundance #52459; Trisiloxane, 1,1,1 5,5,5-hexamethyl-3.3-bis[{trimet 73 147 TBI j 1 ] J I I 11 T* 14 [ I III | 4 281 26.60 26.80 27.00 27.20 5000 m/z 221.05 16.61%

on - 369 m/z~> 50 100 150 200 250 300 350 400 ' ' 450 ‘ Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73 26.60 26.80 27.00 27.20 m/z 74.0.0 8.44% 147 5000 267 355 429 45 207 — miz-> 50 100 150 200 250 300 350 400 450 26.60 26.80 27.00 27.20

28323.D GCMS1126.M Wed Feb 06 13:02:11 2002 Page 11

NYC-WTC_000018535

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NYC-WTC_000018535Source: NYC Law Department, mirrored locally

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