Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
NYC-WTC_000018519–000018545Folder label: “GCMS X 12/18/01 A 12/30/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2701\28323.D Vial: 63 Acq On : 30 Dec 2001 8:55 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 N-(Trifluoroacetyl)-0,0',O'’-t Concentration Rank 4
R.T. EstConc Area Relative to ISTD R.T.
22.79 7.97 ug/1 5633350 Phenanthrene-dl0 24.99
Hit# of 5 Tentative MW MolForm CAS# Qual
1 N-(Trifluoroacetyl^- 0,0',O'’-tris(t 481 C19H34F3NO4Si3 000000-00-0 35 2 Benzeneethanami ne, N-[ (pentafluorop 563 C24H3.4F5NO3Si3 055429-13-5 25 3 N- (Trifluoracetyl)-0,0,0"-tris(tri 495 C20H36F3NO4S13 000000-00-0 25 4 Noradrenaline, tetra-TMS 457 C20H43NO3Si4 000000-00-0 25 Abundance Scan 1933 (22.793 min): 28323.D (-) m/z. 73.00 100.00% 73
5000 147 355 221 281 401 22.40 22.60 22.80 23.00 23.20 m/z~> 04 50 45 - 100 117 17 .191, , ’249 "*"* 150 141.,, 200 250 4 327 300 350 400 450 500 * 441 ■ ■ i ■ ■ ■ ■ i 1 • 1 • i • ‘ 550 m/z 355.05 32.11% Abundance #58326: N-(Trifluoraacetyl)-O,O',O"-tris(trlmethylsilyl)no 73 355 5000 IIIII1ITT-*1*‘+114* 22.40 22.60 22.80 23.00 23.20 m/z 147.00 28.63% 45 120147 193 265 481 ■ ■ i ■ 1 ■ • I ■ 1 ■ ■ i ■ ■ ■ ' i • ‘ -rT-f-r-r-r-r-j-T-r • ■ i * ‘ ■ i ■ ‘ ■ i ■ ■ ■ ■ I ■ ■ ■ • i ■ ' miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine N-Itcentatiugrophenymethiylenej 73 355 2240 22.60 22.80 23.00 23.20 5000 m/z 221.05 20.42%
45 208 251 281 386 458 548 mlz-> ‘50 100 150 200 250 300 350 400 450 500 550 Abundance #58807: N-(Trifluoracetyl)-O,O',O"-tris(trimethyIsilyI)epin 73 22.40 22.60 22.80 23.00 23.20 355 m/z 281.00 16.24% 5000
45 1 140 184 281 480 1 ' 11 1 • l > • • • i • i i • 1 ' ■ i ■ ■ ■ • i ■ ■ ‘ ■ i • ■ 1 1 i ■ ■ ■ ‘ i ' 1 miz-> 50 100 150 200 250 300 350 400 450 500 550 22.40 22.60 22.80 23.00 23.20
28323.D GCMS1126.M Wed Feb 06 13:02:06 2002 Page 10
NYC-WTC_000018534
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NYC-WTC_000018492
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018470
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018287
Analytical notes regarding GCMS scan results and LCS standard recoveries for sample AD30986.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033974
Laboratory report documenting GCMS analysis for unknown compounds and surrogate recovery in sample AD28335 conducted on January 9, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036614
Laboratory comments on GCMS scan results for sample AD29466 noting low recovery and scheduling re-extraction.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018416
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NYC-WTC_000018420
Laboratory report documenting GCMS blank analysis of sample AD30643 conducted on February 1, 2002.
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Laboratory report documenting GCMS reference analysis of sample AD30643 conducted on February 1, 2002.
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