Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
NYC-WTC_000004149–000004492Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2 701\30709.D Vial: 47 Acq On : 30 Dec 2001 4:24 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 7 N-(Trifluoroacetyl)-O,OO 11-t Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T.
22.79 3.36 ug/1 2291900 Phenanthrene-dl0 24.98
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 N-(Trifluoroacetyl)-0,0',O''-tris(t 481 C19H34F3NO4Si3 000000-00-0 37 2 N-(Trifluoracetyl)-0,0',0"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 37 3 Benzeneethanamine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 37 _4 N- (Trifluoro etyl)-N,O,O',0'1-tetr 553 C22H42F3NO4Si4 000000-00-0 35 Abundance Scan 1933 (22.790 min): 30709.D (-) m/z 73.00 100.00% 73
5000 147 355 221 281 327 | 401 22.40 22.60 22.80 23.00 23.20 ii 45 1 ■ 1l 1 TPIT ,1914). 117 249, [ 441............................ m/z 147.00 26.73% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58326: N-(Trifluoroacetyl)-O,O',6"-tris(trimethylsilyl)no 73 355 5000- 22.40 22.60 22.80 23.00 23.20 45 m/z 355.05 26.37% 1I , ■ ' i ' ' 120147 193 265 ..................................... 481.................. m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #53307: N-(Trifluoracetyb)-,00"-tris(trmethylstiy)epin 73 355 22.40 22.60 22.80 23.00 23.20 5000 m/z 221.05 18.70%
45 1 ! 140 184 281 480 m/z- > 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentaf)uoropheny))methylenei 73 355 22.40 22.60 22.80 23.00 23.20 m/z 281.00 14.58% 5000
45 208 251 281 386 458 548 ■ ■ i ' ' m/z-> 50 100 150 200 250 300 350 400 450 500 550 22.40 22.60 22.80 23.00 23.20
30709.D GCMS1126.M Mon Jan 28 11:33:07 2002 Page 7
NYC-WTC_000004316
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28479 analyzed in early December 2001.
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Laboratory report detailing GCMS analysis of sample AD28269 conducted on November 30, 2001.
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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
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Analytical commentary for sample AD28149 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · similarity 0.996
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
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NYC-WTC_000004148
Fragmented OCR text showing dates and identifiers for a DEP GCMS record dated February 2002.
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NYC-WTC_000036712
GCMS analysis report for sample AD29563 listing unknown compounds and surrogate recovery data from January 28, 2002.
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