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Document / 344 pages

DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004149–000004492

Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02

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Scanned page image, NYC-WTC_000004317
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2 701\30709.D Vial: 47 Acq On : 30 Dec 2001 4:24 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 8 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

26.88 1.75 ug/1 1192200 Phenanthrene-dl0 24.98

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 36 2 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 34 3 3-Isopropoxy-1,£,1,7,7,7-hexamethyl 576 C18H52O7Si7 071579-69-6 25 4 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 23 Abundance Scan 2379 (26.885 min): 30709.D (-) m/z 73.00 100.00% 73

5000 147 221 281 26.60 26.80 27.00 27.20 I 0- TT 45 117. , 191, [ 249 [ 327 355,401 429 .................. m/z 147.00 32.52% m/z-> 50 100 150 200 250 300 350 400 450 500 550 (Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147 281 5000 ............................................... 26.60 26.80 27.00 27.20 369 m/z 281.00 16.72% 1 207 249 338 J............................................... --- m/z-> 50100 150 200 250 300 350 400 450 500 550 Abundance -8871: 1-Monolingleoyiglycerl trimethylgily’ ether 73

207 26.60 26.80 27.00 27.20 5000 147 m/z 221.05 15.61% 34 103 281 395 482 m/z-> 50__ 100__ 150 200 250__ 300 350 400 450 500 550 Abundance #60503: 3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim ..........H....... .. 73 26.60 26.80 27.00 27.20 m/z 74.00 8.15% 5000 147

m/z—> 221 281 39— ............. ........ |...... r 327......415.......... 519,561 50 100 150 200 250 300 350 400 A4E

450 500 550 ,,... .s.r.... . , 26.60 26.80 27.00 27.20

30709.D GCMS1126.M Mon Jan 28 11:33:12 2002 Page 8

NYC-WTC_000004317

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NYC-WTC_000004317Source: NYC Law Department, mirrored locally

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