DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2 701\30709.D Vial: 47 Acq On : 30 Dec 2001 4:24 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 9 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

28.65 1.38 ug/1 944396 Phenanthrene-dl0 24.98

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3-Isopropoxy-1,it 1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 40 2 Benzoic acid, -bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 37 3 Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 35 4 1-Monolinoleoylglycerol trimethyl si 498 C27H54O4Si2 054284-45-6 33 Abundance Scan 2571 (28.647 min): 30709.D.(-) m/ z 72.95 100.00% 73

5000 147 221 281 355 ’ 1 1 ' 45 117. 191, 249 1 327 401 429 28.40 28,60 28.80 29.00 TT । r |A i1, । Tit tpmti ■ f t > । । । m/z 147.00 33.41% 50 100 150 200 250 300 350 400 450 500 550 (Abundance #60503: 3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim i 73

5000 147 4 28.40 28.60 28.80 29.00 m/z 221.| 18.39% ‘ ................ ■ l 1 • ■ ■ I ■ ..] 327 . 415 .519561 m/z->50 100 150 200 250 300 350 400 450_ 500 _ 550 Abundance 473975: Beezolo acid 2.4-bisfftrimethyisilyl;axy,- rimet 73 28.40 28.60 28.80 29.00 5000 355 m/z 355.0 15.89% 45 ; 133 193 223 281 s miz-s 50 100 150 200 250 300 350 400 450 500 550 ....................... ....................... [Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methyIene] 73 355 28.40 28.60 28.80 29.00 m/z 281.00 13.54% 5000

45 208 251 281 386 458 548 • ■ I 1 ■ m/z-> 50 100 150 200 250 300 350 400 450 500 550 28.40 28.60 28.80 29.00

30709.D GCMS1126.M Mon Jan 28 11:33:16 2002 Page 9

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