Instrument log and analysis summary for GCMS testing of sample AE09676 conducted on May 23, 2002.
NYC-WTC_000023789–000023810Folder label: “GCMS X 5/9/02 A 5/20/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\MAY2002\9676.D Vial: 10 Acq On : 20 May 2002 4:02 pm Operator: Sample : EXTRACTED 5/9 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 12 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 14
R.T. EstConc Area Relative to ISTD R.T. 29.14 0.83 ug/1 50373 Phenanthrene-dl0 25.52 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Isopropoxy71,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 36 2 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 28 3 2-Hexenedioc acid, bis(trimethylsi 288 C12H2404Si2 055494-10-5 25 4 Benzoic acid. 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 23 Abundance Scan 2630 (29.137 min): 9676.D (-) m/z 73.10 100.00%| 73
.. y... 5000 147 221 281 355 28.80 29.00 29.20 29.40 45 I’ ■ . I 1327I 429 . m/Z 147.05 26.06% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503:3-lsopropoxy-1,1,1 >7.7,7-hexamethyl-3,5,5-tris(trim 73
5000 /y I ' ‘ 'I 1 IT371 1 1 1 1 147 28.80 29.00 29.20 29.40 m/Z 221.10 17.14%| 221 281 327 415 I i. 519 561 m/z—> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73
207 L 28.80 29.00 29.20 29.40 r1 5000 147 rn/z 355.10 15.93%| 34 103 281 ■ ■ ' i 1 ■ 1 ■ i r . I. I , . , , 1 . 395, 482 m/z-> 50 100 150 2(X) 250 300 350 400 450 500 550 Abundance #407/7: 2-Hexenedioic acid, bis(trimethylsilyl) ester, (E)- - 73 28.80 29.00 29.20 29.40 m/z 281.00 11.54%|
5000 147 45
m/z—> 1 n 50 L | 112 100 150 200 244 273 I
250 I
300 350 400 450 500 550 ■ ■ । ■ 1 1 । ■ ' ■ ■ । 1 1 1 11 1 1 1 1 i 1 28.80 29.00 29.20 29.40
9676.D GCMS0520.M Tue May 21 11:39:24 2002 Page 12
NYC-WTC_000023807
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NYC-WTC_000023649
Laboratory report showing GC/MS blank analysis for sample AE09676 with non-detect results for volatile organic compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039588
Laboratory report documenting GCMS analysis of sample AE06455 conducted on April 19, 2002, by the DEP.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005394
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02604.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009835
Calibration data for GCMS analysis using 625/TCLP method with deuterated compound reference standards recorded on February 21, 2002.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038871
Laboratory report documenting GCMS analysis of sample AE02575 conducted on March 25, 2002, identifying other unknown compounds.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039497
Laboratory report documenting GCMS analysis of sample AE06449 conducted on April 19, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005415
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02645.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039469
Laboratory report documenting GCMS analysis of sample AE06430 conducted on April 19, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005367
Laboratory report showing non-detectable results for nitrosamines and chlorinated solvents in GCMS blank.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047979
GCMS analysis report for sample AE05749 showing surrogate recovery and unknown compounds from April 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013943
TCLP calibration table document dated May 24, 2002, listing deuterated standards and response factors for GCMS analysis.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039611
Laboratory report documenting GCMS analysis of sample AE06456 conducted on April 19, 2002, by the DEP.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000023646
Department of Environmental Protection administrative record sheet for World Trade Center site activities dated May 2002.
Filed in the same folder
NYC-WTC_000023647
Technical data file header page from a GCMS analysis run associated with the World Trade Center site in May 2002.
Filed in the same folder
NYC-WTC_000023649
Laboratory report showing GC/MS blank analysis for sample AE09676 with non-detect results for volatile organic compounds.
Filed in the same folder
NYC-WTC_000023662
Laboratory report showing GC/MS calibration data for volatile organic compounds analyzed on May 20-21, 2002.
Filed in the same folder
NYC-WTC_000023666
Laboratory report showing GC/MS reference analysis for sample AE09676 with quantitative results for volatile organic compounds.
Filed in the same folder