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GCMS analysis results for sample AE02647, Mar 15, 2002

Machine-extracted title · confidence 90%

Laboratory report listing unknown compounds and surrogate recovery data for sample AE02647.

NYC-WTC_000005448–000005462

Folder label: “GCMS X 2/5/02 A 3/7/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\1\DATA\MAR0 7 02\2647.D Vial: 20 Acq On 8 Mar 2002 8:25 am Operator: Sample gc/ms scan 2/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 7 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

25.59 0.23 ug/1 41574 Phenanthrene-dl0 25.69

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Isopropoxy-1, 1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 43 2 1,1,1,5,7,7,/-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 40 3 1 -Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 25 4 3-TrimethyIsilyloxystearic acid, tr 444 C24H5203Si2 000000-00-0 9 Abundance Scan 2238 (25.587 min): 2647.D (-) • m/ z 73.00 100.00% 73

5000 147 - 221 281 355 429 j 25.20 25.40 25.60 25.80 26.00 45 TT +-4417 V " , I . 3251,% 401 — — 1 r m/ z 14 7.0.0 34.30% m/z->.... 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-sopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73

5000 ‘ i ' ' ' ' i ' ' ' ■ i ' ■ 147 : 25.20 25.40 25.60 25.80 26.00 , 7. m/z 221.05 25.86% ..... !...... ...... . .............................. . 561 m/z->_... 50 100 150 200 250 300 350 400 450 500 550 j Abundance ■ । 73 ......................... ,.................................

147 25.20 25.40 25.60 25.80 26.00 5000- 267 m/z 429.15 15.11% 355 429 45 207

. 50 100 150 200 250 300 350 400 450 500 550 Abundance #58871: 1-Monolinoleoyigiycerol trimethylsilyl ether ■ i ■ ' i ■ ■ ■ ■ । • i ■ • 73 25.20 25.40 25.60 25.80 26.00 m/z 355.05 12.72% 207 5000- 147 34 103 281 .1 .. ...395.. 482.... 1 i ■ ■ ■ ■ i ■ ' i ■ ■ ■ • । 1 । 1 ■ j ■ > m/z-> 50 100 150 200 250 300 350 400 450 500 550 25.20 25.40 25.60 25.80 26.00

2647.D GCMS0208.M Wed Mar 13 14:58:40 2002 Page 7

NYC-WTC_000005461

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NYC-WTC_000005461Source: NYC Law Department, mirrored locally

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