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GCMS analysis results for sample AE02645, Mar 15, 2002

Machine-extracted title · confidence 90%

Laboratory report listing unknown compounds and surrogate recovery data for sample AE02645.

NYC-WTC_000005415–000005434

Folder label: “GCMS X 2/5/02 A 3/7/02

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Scanned page image, NYC-WTC_000005428
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\l\DATA\MAR0702\2645.D Vial: 18 Acq On 8 Mar 2002 6:27 am Operator: Sample gc/ms scan 2/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 7 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

25.59 0.47 ug/1 90734 Phenanthrene-dl0 25.69

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3 -Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 43 2 1,1,1,5,7,7, 7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 17 3 Mesoxalic /acid-2-trifluoroacetamido 447 C14H28F3NO6Si3 042827-96-3 10 4 Benzoic acid, 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 9 Abundance Scan 2238 (25.590 min): 2645.D (-) m/ z 73.00 100.00% 73

5000 147 221 | 281 355 429 45 191 | [ 249 | 325 401 25.20 25.40 25.60 25.80 26.00

m/z-> 1 ''i ' ■ 50 117 ' 1 1 1 1 r 1 100 150 1 1 1 ' i ‘ 200 250 300 —1 ■ i ' ' 1 1' I 1 1 350 400 ' I ' 1 450 500 .1............... 550 m/z 147.00 30.97% Abundance #60503: 3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73

......................... /.................. ..... 5000 147 25.20 25.40 25.60 25.80 26.00 221 m/z 221.05 22.65% 281 327 415 519 561 m/z-. _ 50 100 150 200 250 11110a 300 350 400 450 500 550 Abundance 73

147 25.20 25.40 25.60 25.80 26.00 5000 267 m/z 429.15 14.60% 355 429 45 207

m/z-> 50 100 150 200 250 300 350 400 450 500 550 ......................... ,.................................. Abundance #56914: Mesoxalic acid-2-trifluoroacetamido-, tri(trimethyl 73 25.20 25.40 25.60 25.80 26.00 m/z 355.05 14.18% 5000 147 190

m/z-> 120 1 1 I 1 1 1 1T1 1 1 50 100 150 200 258 300 250 350 400 2 450 500 550 25.20 25.40 25.60 25.80 26.00

2645.D GCMS0208.M Wed Mar 13 14:54:30 2002 Page 7

NYC-WTC_000005428

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NYC-WTC_000005428Source: NYC Law Department, mirrored locally

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