NYC-WTC_000005415
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02645.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗Document / 21 pages
GCMS analysis results for sample AE02604, Mar 15, 2002
Machine-extracted title · confidence 90%Laboratory report listing unknown compounds and surrogate recovery data for sample AE02604.
NYC-WTC_000005394–000005414Folder label: “GCMS X 2/5/02 A 3/7/02”
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NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\l\DATA\MAR0702\2604.D Vial: 17 Acq On 8 Mar 2002 5:28 am Operator: Sample gc/ms scan 2/5 fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 9 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 8
R.T. EstConc Area Relative to ISTD R.T.
27.52 0.31 ug/1 61599 Phenanthrene-dl0 25.69
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3 -Isopropoxy-1,1,1, 7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 45 2 Ethanedioic aci d, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 38 3 Trisiloxane, 1, ,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 25 4 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 25 Abundance Scan 2448 (27.517 min): 2604.D (-) | m/z 73.00100.00% 7b
5000 147 221 281 . .. 4... .. 27.20 27.40 27.60 27.80 45 — ■ | 117 > 1 19| . ..327,355 ..... ............... 420 450 ' I ' ' 1 f I ' ■ ' ‘ I ' ' r ' I ' 1 ' ' I ' ' 1 ' I ' 1 T 1 I ' ' ' ' I * 1 ' 1 I ' ' m/z 147.00 36.86% m/z-_ Abundance 50 100 150 200 250 300 350 400 500 550 #60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73
5000 147 27.20 27.40 27.60 27.80 221 m/z 221.05 18.61% 281 327 415 519 561 m/z-->__ 50 100 150 200 250 300 350 400 450 500 550 Abundance 73 147
27.20 27.40 27.60 27.80 5000 m/z 281.00 18.43% 45 190 219
m/Z-? _ 50 100 150 200 250 300 350 400 450 500 550 Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147 27.20 27.40 27.60 27.80 281 m/z 207.0.0 9.13% 5000
369 , 297 249, m/z-> ------------- 50 100 150 200 250 I 338 I 1 ' l ' ' ’ 1 I r ' ‘ ' I 1 1 1 1 I Ti i t- | ti i i | i i 300 350 400 450 500 550 T-T-i-T-r-r-r-f -A- 27.20 27.40 27.60 27.80
2604.D GCMS0208.M Wed Mar 13 14:51:09 2002 Page 9
NYC-WTC_000005409
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