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GCMS analysis results for sample AE02604, Mar 15, 2002

Machine-extracted title · confidence 90%

Laboratory report listing unknown compounds and surrogate recovery data for sample AE02604.

NYC-WTC_000005394–000005414

Folder label: “GCMS X 2/5/02 A 3/7/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\1\DATA\MARO7O2\26O4.D Vial: 17 Acq On 8 Mar 2002 5:28 am Operator: Sample gc/ms scan 2/5 fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

29.29 0.26 ug/1 51920 Phenanthrene-dl0 25.69

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 37 2 3-Isopropoxy-1,1/1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 25 3 Ethanedioic aci , bis(trimethylsily 234 C8H18O4Si2 018294-04-7 16 4 Noradrenaline,/ tetra-TMS 457 C20H43NO3Si4 000000-00-0 16 Abundance Scan 2641 (29.289 min): 2604.D (-) m/ z 73.00100.00% 73

5000- 147 221 355 ................... . 281 29.00 29.20 29.40 29.60 45 ----- 11/ -| m/z 147.00 401 429 TT 41.42% m/z-> 50 100 150 200 250 300 400 350 450 500 550 1 Abundance #52459: f risiloxane, 1,1,1,5,5,5-hexamethyi-3,3-bis[(trimet

73 147

281 ................ /, 5000 29.00 29.20 29.40 29.60 369 m/z 355.05 32.06% 207 249, m/z-50 Ti ' । 1 ' 1 1 1 ' ' 100 150 1 11 [ 200 H 250 300 338 . | , , , , , ............ ... 350 400 450 500 550 Abundance 73 ........... /...................... 29.00 29.20 29.40 29.60 5000 147 m/z 221.05 27.80%

221 281 327 415 519 561 1 * i > * m/z-2 50 100 150 200 250 300 350 400 450 500 550 Abundance #30580: Ethanedioic acid, bis(trimethylsilyl) ester /........ 73 147 29.00 29.20 29.40 29.60 m/z 281.10 24.17% 5000 45

I i t . 190 219 - m/z~> 50 100 150 200 250 300 350 400 450 500 550 29.00 29.20 29.40 29.60

2604.D GCMS0208.M Wed Mar 13 14:51:14 2002 Page 10

NYC-WTC_000005410

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NYC-WTC_000005410Source: NYC Law Department, mirrored locally

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