GCMS calibration analysis results, DEP Labs, Feb 2002

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Data File : C:\HPCHEM\1\DATA\FEB2102\472.D Vial: 6 Acq On : 21 Feb 2002 7:01 pm Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

27.56 0.34 ug/1 30732 Phenanthrene-dl0 25.73

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3 - Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 56 2 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 47 3 1-Monolinoleoylglycerol/trimethylsi 498 C27H5404Si2 054284-45-6 39 4 2-Hexenedioic. acid, bis(trimethylsi 288 C12H2404Si2 73.00....100.00% Scan 24594274558mn2472.06) 055494-10-5 35 Abundance 73 m/z

5000 147 221 281 40 . . 327,355 .. 429 27.20 27.40 27.60 27.80

m/z-> 1 150' 'I -------------- m/z 147.00 34.51% 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3.5,5-tris(trim 73

- 5000 147 27.20 27.40 27.60 27.80 221 281 m/z 281.00 18.53% ................... 7... 0. , 415 519 561 m/z->____ 50 100 150 200 250 300 350 400 450 500 550 Abundance 73 147 • i ■ ' ' • i ' ‘ i ‘ ' i ' 281 27.20 27.40 27.60 27.80 5000 rn/z 221.05 16.49% 369 207 249 338 **I/*//*I4*I***II4*’/I4I*IIIIIIIIIIIIIIIIIII m/z-> 50 100 150 200__ 250 __ 300 __350 . 400 450. 500 550 Abundance #58871:1-Monolinoieoyiglycerol trimethylsilylether 73 27.20 27.40 27.60 27.80 m/z 39.95 7.86% 207 5000 147 34 103 281 395 I (,, ,1 i . 482 m/z-> 50 100 150 200 250 300 350 400 450 500 550 27.20 27.40 27.60 27.80 '

472.D GCMS0208.M Fri Feb 22 09:42:43 2002 Page 8

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