NYC-WTC_000009619
Calibration table page listing internal standards and response factors for GCMS analysis.
Same agency, volume and box · similarity 0.993
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GCMS calibration analysis results, DEP Labs, Feb 2002
Machine-extracted title · confidence 100%Calibration data for GCMS analysis using 625/TCLP method with deuterated compound reference standards recorded on February 21, 2002.
NYC-WTC_000009835–000009850Folder label: “GCMS X 1/22/02 A 2/22/02”
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NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\FEB2102\472.D Vial: 6 Acq On : 21 Feb 2002 7:01 pm Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
25.63 0.46 ug/1 42168 Phenanthrene-dl0 25.73
Hit# of 5 Tentative ID MW MolForm CAS# Qual
l l,l,l,5,7,7,7-H0tamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 50 2 3-Isopropoxy-1/1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 37 3 N-Met hyl adrenaline, tri-TMS 413 C19H39NO3Si3 000000-00-0 10 4 3-TrimethylsJ yloxystearic acid. tr 444C24H52O3Si2 000000-00-0 9 Abundance Scan 2243 (25.631 min): 472.D (-)' | m/z 73.00 100.00% 73
5000- 147 221 281 355 429 25.40 25.60 25.80 26.00 45 i 'Y t r ________ _______ I __ _ _132511401 ' • i ■ ' ' ' i • ■ ■ ‘ i ' ■ ' ■ 1 ' ' f ■ i ■ ' • ' i ■ ‘ ■ f ‘ ‘ 1 ‘ i ■ ■ ■ ■ i ‘ ' m/z 147.00 32.23% m/z-> 50 100 _150 200 _ 250 300 350 400 450 500 550 Abundance #56714: 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73
5000 147 267 355 429 A.. . 25.40 25.60 25.80 26.00 45 207 m/z 221.05 22.44% ----- m/z->____ 50_ 100 150 200 250 300 350 400 450 500 550 Abundance - 73 ......................... ............................
25.40 25.60 25.80 26.00 5000 147 m/z 429.05 17.30% 221 281 327 415 519 561 m/z->__ 50....... 100..... .150 __ 200...... 250 .. 300 __ 350...... 400... 450 .... 500...... 550 Abundance #54808: N-Methyladrenaline, tri-TMS ' 1 1 ' 1 1 ' I 1 1 1 1 I1 1 ' I ' ' 73 25.40 25.60 25.80 26.00 m/z 355.05 14.47% 5000 355 45 207 267 323 ' ’I ' ' ‘ 1 । ■ * ■ ■ । ■ , 1 ,, I, 1 1 i 1 ■ 1 1 r1 ' • 1 i 1 1 ' 1 i 1 1 m/z-> 50 100 150 200 250 300 350 400 450 500 550 25.40 25.60 25.80 26.00
472.D GCMS0208.M Fri Feb 22 09:42:38 2002 Page 7
NYC-WTC_000009845
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