NYC-WTC_000005415
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02645.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗Document / 21 pages
GCMS analysis results for sample AE02604, Mar 15, 2002
Machine-extracted title · confidence 90%Laboratory report listing unknown compounds and surrogate recovery data for sample AE02604.
NYC-WTC_000005394–000005414Folder label: “GCMS X 2/5/02 A 3/7/02”
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NYC 9/11 Public Portal Document Library Search Compound Report
Data File C:\HPCHEM\l\DATA\MAR0702\2604.D Vial: 17 Acq On 8 Mar 2002 5:28 am Operator: Sample gc/ms scan 2/5 fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 1,1,1,5,7,7,7-Heptamethyl-3,3 - Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
25.59 0.43 ug/1 85836 Phenanthrene-dl0 25.69
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 36 2 3-Isopropoxy-1,1,1/7,7,7-hexamethyl 576 C18H52O7Si7 071579-69-6 32 3 IH-Pyrimido[4,5,&Zij][2,7]naphthyri 283 C14H13N5O2 055044-48-9 9 4 3-Trimethylsilyloxystearic acid, tr 444 C24H52O3Si2 000000-00-0 9 Abundance Scan 2238 (25.589 min): 2604.D (-) m/ z 73.00 100.00% 73
5000 147 221 20- 355 429
m/z-> 45 —T 50 117 100 150 191 | 200 —4 250 300 350 400 450 500 550 25.20 25.40 25.60 25.80 26.00 m/z 147.00 31.08% Abundance #56714: 1.1.1.5.7.7.7-Heptametnyl-3,3-bis(trin'ethylsiloxy)t 73
5000 147 267 / N 355 429 25.20 25.40 25.60 25.80 26.00 45 207 m/z 221.05 22.11% 1 -
m/z-> . _ 50 100 150 200 250 300 350 400 450 500 550 Abundance 73
25.20 25.40 25.60 25.80 26.00 5000 147 m/z 429.15 13.29%
221 281 327 415 519 561 50 100 150 200 250 300 350 400 450 500 550 Abundance #39933:1 H-Pyrimido[4,5.6-ij][2,7]naphthyridine-6-carbonitr
44 73 25.20 25.40 25.60 25.80 26.00 m/z 355.05 13.03% 5000
m/z-> A t4 50 100 150 200 250 300 350 400 450 500 550 25.20 25.40 25.60 25.80 26.00
2604.D GCMS0208.M Wed Mar 13 14:51:00 2002 Page 7
NYC-WTC_000005407
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NYC-WTC_000005407Source: NYC Law Department, mirrored locally
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