NYC-WTC_000005394
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02604.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Document / 16 pages
GCMS blank analysis results, Mar 13, 2002
Machine-extracted title · confidence 90%Laboratory report showing non-detectable results for nitrosamines and chlorinated solvents in GCMS blank.
NYC-WTC_000005367–000005382Folder label: “GCMS X 2/5/02 A 3/7/02”
Page image
OCR text
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\MAR0 7 0 2\LB.D Vial: 15 Acq On 8 Mar 2002 3:29 am Operator: Sample gc/ms scan 2/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 7 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 7
R.T. EstConc Area Relative to ISTD R.T.
25.58 0.30 ug/1 51181 Phenanthrene-dl0 25.69
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 l,l,l,5,7,7,7-Heptanfethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 47 2 3 -Isopropoxy-1,1, <7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 25 3 3-Trimethylsilyla ystearic acid, tr 444 C24H5203Si2 000000-00-0 17 4 N-Methyladrenaline, tri-TMS 413 C19H39NO3Si3 000000-00-0 12 Abundance Scan 2237 (25.584 min): LB.D (-) m/z 73.0,0 ' 100.00% 73 / ।
5000 147 221 281 | 355 429 25.20 25.40 25.60 25.80 26.00 45 1’11 t . 1911 L ■ , ■ I, 325,1 . . 401 3....................... m/z 147.0,0 32.54% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #56714: i,1,1,5,7,7,7-Heptamethyi-3,3-bis(trimethylsiloxy)t 73
5000 147
207 267 355 429 . A. 25.20 25.40 25.60 25.80 26.00 45 m/z 221.05 22.86%
m/z->50___ 100 150 200 250 300 350 400 ' 450 500 550 Abundance 73 TI i ■ ■ ■ 1 i ■ 25.20 25.40 25.60 25.80 26.00 5000 m/z 355.05 12.53% 147
221 281 327 415 519 561 ‘ ■ i ■ ' ' ■ i ' m/z-> 50 100 ..150__ 200 __250 300 350 400 450_ 500 550 Abundance #56734: 3-Trimethyisilyloxystearic acid, trimethylsilyl est .................. | I.................. 73 25.20 25.40 25.60 25.80 26.00 m/z 281.0.0 9.82% 5000 147 233
313 429 189
m/z-> 50 100 150 200 -L397 250 300 350 400 ' ' 450 ' ' 500 550 ■ ■ i • • ■ i ■ • ■ ■ i ' ■ 1 1 । 1 1 1 1 i 1 1 1 1 i 1 25.20 25.40 25.60 25.80 26.00
LB.D GCMS0208.M Wed Mar"13 15:04:00 2002 Page 7
NYC-WTC_000005379
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NYC-WTC_000005379Source: NYC Law Department, mirrored locally
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