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GCMS blank analysis results for sample AE09447, May 2002

Machine-extracted title · confidence 100%

GCMS blank analysis report for sample AE09447 listing compounds below detection limits from May 8, 2002.

NYC-WTC_000045400–000045410

Folder label: “GCMS X 5/3/02 A 5/8/02

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Scanned page image, NYC-WTC_000045407
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\MAY0802\LB.D Vial: 3 Acq On 8 May 2002 11:33 am Operator: Sample GC/MS SCAN 5/3 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0507.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 2 1,1,1,5,7,7,7-Heptamethyl-3,3 - Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T.

25.48 0.46 ug/1 38588 Phenanthrene-dl0 25.57 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 l,l,l,5,7/7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 39 2 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 25 3 1 -Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 9 4 Prost-13fr-en-l-oic acid, 9-(methoxyi 599 C30H61NO5Si3 039062-24-3 9 Abundance Scan 2231 (25.481 min): LB.D (-) m/ z 73.10 100.00% 73

5000 147 / 221 i 1 1 ' ' i 281 355 429 25.20 25.40 25.60 25.80 45 11 . . " , 325,1 401 1 ................... m/z 147.05 25.37% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73

147 5000 267 A) 1 ' । 1 1 25.20 25.40 25.60 25.80 355 429 45 207 m/z 221.10 17.37%

' 1 i 1 । 1 1 1 ‘ । 1 ■ * 1 । 1 1 m/z—> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503:3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73

25.20 25.40 25.60 25.80 5000 m/z 429.05 12.13% 147

221 201 327 I 415 519 561 ’ III’1111111 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether ....... ,....... 73 25.20 25.40 25.60 25.80 m/z 355.10 10.66% 207 5000 147

34 103 281

m/z—> 50 100 150 200 1. 250 300 350 395, 400 450 , 482 500 550 , . 1.. 25.20 25.40 25.60 25.80

LB.D GCMS0507.M Thu May 09 14:43:51 2002 Page 2

NYC-WTC_000045407

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NYC-WTC_000045407Source: NYC Law Department, mirrored locally

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