NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\l\DATA\MAY0802\LB.D Vial: 3
Acq On 8 May 2002 11:33 am Operator:
Sample GC/MS SCAN 5/3 Inst : 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0507.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
Peak Number 2 1,1,1,5,7,7,7-Heptamethyl-3,3 - Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T.
25.48 0.46 ug/1 38588 Phenanthrene-dl0 25.57
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 l,l,l,5,7/7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 39
2 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 25
3 1 -Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 9
4 Prost-13fr-en-l-oic acid, 9-(methoxyi 599 C30H61NO5Si3 039062-24-3 9
Abundance Scan 2231 (25.481 min): LB.D (-) m/ z 73.10 100.00%
73
5000
147 /
221 i 1 1 ' ' i
281 355 429 25.20 25.40 25.60 25.80
45
11 . . " , 325,1 401 1 ................... m/z 147.05 25.37%
m/z-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t
73
147
5000 267 A) 1 ' । 1 1
25.20 25.40 25.60 25.80
355 429
45 207 m/z 221.10 17.37%
' 1 i 1 । 1 1 1 ‘ । 1 ■ * 1 । 1 1
m/z—> 50 100 150 200 250 300 350 400
450 500 550
Abundance #60503:3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim
73
25.20 25.40 25.60 25.80
5000 m/z 429.05 12.13%
147
221 201 327
I 415 519 561
’ III’1111111
m/z-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether ....... ,.......
73 25.20 25.40 25.60 25.80
m/z 355.10 10.66%
207
5000 147
34 103
281
m/z—> 50 100 150 200
1.
250 300 350
395,
400 450
, 482
500 550
, . 1..
25.20 25.40 25.60 25.80
LB.D GCMS0507.M Thu May 09 14:43:51 2002 Page 2
NYC-WTC_000045407
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