NYC-WTC_000039588
Laboratory report documenting GCMS analysis of sample AE06455 conducted on April 19, 2002, by the DEP.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Document / 20 pages
GCMS analysis results for sample AE02575, March 2002
Machine-extracted title · confidence 90%Laboratory report documenting GCMS analysis of sample AE02575 conducted on March 25, 2002, identifying other unknown compounds.
NYC-WTC_000038871–000038890Folder label: “GCMS X 3/4/02 A 3/20/02”
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NYC 9/11 Public Portal Document Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\MAR1902\2575.D Vial: 24 Acq On : 21 Mar 2002 3:41 am Operator: Sample : gc/ms scan 3/4 Inst : GC/MS 2 09 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0308 .M (RTE Integrator) Title : 209 625/TCLP calibration table Library- : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 7
R.T. EstConc Area Relative to ISTD R.T.
25.56 0.39 ug/1 83815 Phenanthrene-dl0 25.66
Hit# of 5 Tentative ID MW MolForm CAS# Qual ______________________ /______________________________________________ 1 1,1,1,5,7,7,7-Heptamethy1-3,3-bis(t 444 C13H40O5Si6 038147-00-1 39 2 3-TrimethylsilJloxystearic acid, tr 444 C24H5203Si2 000000-00-0 17 3 Silanamine, N-(2,6-dimethyl-4-[(tri 281 C14H27NOSi2 072088-09-6 9 4 1H-Pyrimido [4 , ,6-ij][2,7]naphthyri 283 C14H13N5O2 055044-48-9 9 Abundance Scan 2234 (25.558 min): 2575.D (-) m/ z 73.00 100.00% . 73
5000 147 221 ...... —.... 281 355 429 25.20 25.40 25.60 25.80 45 TTHTT 117 , 191 | , TTDP] 249 | 325..... 401 ...1 IT"OITTETEt—BI—M[T m/z 147.00 33.36% m/z-> 40 60 80 100120140160 180 200 220 240 260 280300 320 340 360 380 400 420 Abundance #56714: 1.1,1,5,7,7,7-Heptamethyi-3,3-bis(trimethylsiioxyjt 73
5000 147 267 / A 355 429 25.20 25.40 25.60 25.80 45 207 m/z 221.05 21.24% . 1 TTT[ 11’1111111111111111111111111111111101111111111111111111011111—111011111 m/z-> 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance oet 0 0 ii " 7 " gm ptpuytytgym 73
25.20 25.40 25.60 25.80 147 233 5000 m/z 355.05 14.93% 313 429 189 387 339 m/z-> ...... 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance #39584: Silanamine, N-[2,6-dimethy/-4-[(trimethylsilyl)oxy] ...................... —......................... — 73 25.20 25.40 25.60 25.80 281 m/z 429.15 14.91% 209 5000 45 251 147 179
m/z-> +-25,,474 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 ' i ' ' 25.20 25.40 25.60 25.80 ■ । r 1 ■ ' । ■ ■ ‘ ■ । ■
2575.D GCMS0308.M Thu Mar 21 14:23:50 2002 Page 7
NYC-WTC_000038884
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