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GCMS analysis results for sample AE02575, March 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AE02575 conducted on March 25, 2002, identifying other unknown compounds.

NYC-WTC_000038871–000038890

Folder label: “GCMS X 3/4/02 A 3/20/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR1902\2575.D Vial: 24 Acq On : 21 Mar 2002 3:41 am Operator: Sample : gc/ms scan 3/4 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 6 Benzeneethanamine, N-[(pentafl Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

23.38 0.51 ug/1 112324 Acenaphthene-dl0 21.22

Hit# of 5 /Tentative ID MW MolForm CAS# Qual L--------- 1 Benzeneethanamine, N- [ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 43 2 Phenethylamine, N-methyl-.beta. , 3,4 3 99 C18H3 7NO3Si3 010538-85-9 43 3 Benzoic acid, 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 38 4 N-(Trifluoroacetyl)-N,O,OO1'-tetr 553 C22H42F3NO4Si4 000000-00-0 38 Abundance Scan 1997 (23.382 min): 2575.D (-) m/ z 73.0.0 100.00% (

5000 355 147 —....... ...... ...... 221 281 45 401 23.00 23.20 23.40 23.60 23.80 117. 191 249 . [ 327 — 1 'i 1 ‘ 1 i ' 1 1 1 i ' 1 1 1 i ' ' > ■ l 1 ■ > > I ■ 1 • 1 l • ■■ । I ■— m/z 355.05 41.88% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-Kpentafluoropheny)methylene] 73 355

..... —........... 5000 23.00 23.20 23.40 23.60 23.80 45 m/z 147.00 31.02% LL L ... 208 251 281 ■ ■ i ■ ■ • ■ । ■ ■ ■ ■ । (386 ■ । > । । । 458 548 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance ■ .: 73 ...... 23.00 23.20 23.40 23.60 23.80 5000 355 m/z 221.05 24.43% 44 147 193 267294 m/z->...... ..... 50_100.... 150_ 200 250 300 350 400 450 500 550 Abundance #73975: Benzoic acid, 2,4-bis[(trimethyisilyl)oxy]-, trimet 73 23.00 23.20 23.40 23.60 23.80 m/z 281.00 16.91% 5000 355 45

TII—PTT r ."l 133 193 223 T T । ,T 281 |% । । । । । । । I T । i ! 7 । । । I TII I ........... 4............. m/z-> 50 100 150 200 250 300 350 400 450 500 550 23.00 23.20 23.40 23.60 23.80

2575.D GCMS0308.M Thu Mar 21 14:23:45 2002 Page 6

NYC-WTC_000038883

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NYC-WTC_000038883Source: NYC Law Department, mirrored locally

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