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Document / 344 pages

DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004149–000004492

Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02

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Scanned page image, NYC-WTC_000004484
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB1302\30648.D Vial: 14 Acq On : 14 Feb 2002 3:48 am Operator: 209 GALOS Sample : GC/MS SCAN Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L **************************************************** ** * * * * * * * ****** * * Peak Number 7 Benzeneethanamine, N-[(pentafl Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

23.47 1.14 ug/1 539475 Acenaphthene-dl0 21.32

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzeneethanamine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 43 2 Trisiloxane, 1,1,1,5,5,5-h^xamethyl 384 C12H3604Si5 003555-47-3 37 3 N- (Trifluoracetyl) -0,0-tris (tri 495 C20H36F3NO4Si3 000000-00-0 37 4 N-(Trifluoroacetyl)-N,0,0‘,0'1-tetr 553 C22H42F3NO4Si4 000000-00-0 35 Abundance Scan 2007 (23.465 min): 30648.D (-) m/ Z 73.00 100.00% 73

5000 147 355 -- 221 281 45 191 [ 249 [ 327 | 401 23.20 23.40 23.60 23.80 — 117. L ITT m/z 147.00 25.97% m/z~> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafiuorophenyljmetFiylene] 73 355

5000 23.20 23.40 23.60 23.80 45 m/z 355.05 24.73% 208 251 281 | 386 458 548 miz->__ 50 100 150 200 250 300 350 400 450 500 550 Abundance 73 147 ............... 281 23.20 23.40 23.60 23.80 5000 m/z 221.05 17.96%

207 369 ,249 .... 338 ................ m/z--> 50 100 150 200 250 300 350 400 450 500 550 ...... .... ..... .. Abundance #58807: N-(Trifluoracetyl)-O,O',O"-tris(trimethylsiiyl)epin 73 23.20 23.40 23.60 23.80 355 m/z 281.00 16.96% 5000

, 45r, । 1 '1 1 ‘ ii 140 1 ‘ ‘ i 1 1 184 281 । 480 ' 1 i * 1 > ' । 1 1 *' 1 i 1 1 1 1 i 1 1 1 1 I 1 1 1 1 I 1 -T-|-r-|-r-r-r-r-|-r-r . .... .......... .. m/z-> 50 100 150 200 250 300 350 400 450 500 550 23.20 23.40 23.60 23.80

30648.D GCMS0103.M Thu Feb 14 11:01:48 2002 Page 7

NYC-WTC_000004484

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NYC-WTC_000004484Source: NYC Law Department, mirrored locally

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