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Document / 344 pages

DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004149–000004492

Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02

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Scanned page image, NYC-WTC_000004485
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB1302\30648.D Vial: 14 Acq On : 14 Feb 2002 3:48 am Operator: 209 GALOS Sample : GC/MS SCAN Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 3-Isopropoxy-l,1,1,7,7,7-hexam Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

25.64 0.81 ug/1 384319 Phenanthrene-dl0 25.77

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 36 2 2-Hexenedioic acid, bis(trimethylsi 288 C12H2404Si2 055494-10-5 32 3 Ethanedioic acid, bis (trimethylsily 234 C8H18O4Si2 018294-04-7 32 4 Silane, [(1-methoxy-l,3-propanediyl 250 C10H26O3Si2 062185-57-3 23 Abundance Scan 2244 (25.641 min): 30648.D (-) m/ z 73.0,0 100.00% 73

5000 147 221 ..... ——...... . . 281 25.40 25.60 25.80 26.00 45 TTmBdnom 191 117 I 249 [ 325, 355 [ 401 429 ■ ■1i ■ ITIT rM 1 ' I 1 1 1 1 I ' TTT m/z 147.00 26.26% m/z—>.... 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73

5000 147 .25.40 /.M .....25.60 ....... 25.80 26.00

221 m/ z 221.05 16.36% 281 327 415 519 561 — , I III**IIIIII* m/z->50 100__ 150 200 250 300 350 400 450 500 550 Abundance 73

25.40 25.60 25.80 26.00 5000 m/z 355.05 8.80% 147 45

; 112 244 273 m/z—?_ Abundance 50 73 100 150 200 250 300 350 400 #30580: Ethanedioic acid, bis(trimethylsilyi) ester 147 450 500 550 .... /r----— 25.40 25.60 25.80 26.00 m/z 281.00 8.79% 5000 45

m/z-> . Il.. 1 1 i ' ■ ■ ■ i ' ' 50 100 150 219 200 250 300 350 400 450 500 550 m 25.40 25.60 25.80 26.00

30648.D GCMS0103.M Thu Feb 14 11:01:52 2002 Page 8

NYC-WTC_000004485

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NYC-WTC_000004485Source: NYC Law Department, mirrored locally

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