NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\FEB1302\30648.D Vial: 14
Acq On : 14 Feb 2002 3:48 am Operator: 209 GALOS
Sample : GC/MS SCAN Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 8 3-Isopropoxy-l,1,1,7,7,7-hexam Concentration Rank 7
R.T. EstConc Area Relative to ISTD R.T.
25.64 0.81 ug/1 384319 Phenanthrene-dl0 25.77
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 36
2 2-Hexenedioic acid, bis(trimethylsi 288 C12H2404Si2 055494-10-5 32
3 Ethanedioic acid, bis (trimethylsily 234 C8H18O4Si2 018294-04-7 32
4 Silane, [(1-methoxy-l,3-propanediyl 250 C10H26O3Si2 062185-57-3 23
Abundance Scan 2244 (25.641 min): 30648.D (-) m/ z 73.0,0 100.00%
73
5000
147
221 ..... ——......
. . 281 25.40 25.60 25.80 26.00
45
TTmBdnom 191
117 I 249 [ 325, 355
[ 401 429
■ ■1i ■
ITIT rM 1 ' I 1 1 1 1 I ' TTT m/z 147.00 26.26%
m/z—>.... 50 100 150 200 250 300 350 400 450 500 550
Abundance #60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim
73
5000
147
.25.40 /.M
.....25.60 .......
25.80 26.00
221
m/ z 221.05 16.36%
281 327 415 519 561
— , I
III**IIIIII*
m/z->50 100__ 150 200 250 300 350 400 450 500 550
Abundance
73
25.40 25.60 25.80 26.00
5000 m/z 355.05 8.80%
147
45
; 112 244 273
m/z—?_
Abundance
50
73
100 150 200 250 300 350 400
#30580: Ethanedioic acid, bis(trimethylsilyi) ester
147
450 500 550
.... /r----—
25.40 25.60 25.80 26.00
m/z 281.00 8.79%
5000
45
m/z->
. Il..
1 1 i ' ■ ■ ■ i ' '
50 100 150
219
200 250 300 350 400 450 500 550
m
25.40 25.60 25.80 26.00
30648.D GCMS0103.M Thu Feb 14 11:01:52 2002 Page 8
NYC-WTC_000004485
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