Instrument log and analysis summary for GCMS testing of sample AE09676 conducted on May 23, 2002.
NYC-WTC_000023789–000023810Folder label: “GCMS X 5/9/02 A 5/20/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\l\DATA\MAY2002\9676.D Vial: 10 Acq On : 20 May 2002 4:02 pm Operator: Sample : EXTRACTED 5/9 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 13 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 30.73 1.27 ug/1 44759 Chrysene-dl2 33.57 Hit# of 5 Tentative ID MW MolForm CAS# Qual
l l,l,l,5,7/7,7yHeptamethyl-3,3-bis(t 444 C13H40O5S16 038147-00-1 50 2 Silanamine, N- [2,6-dimethyl-4-[(tri 281 C14H27NOSi2 072088-09-6 25 3 3-Isopropoxy/1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 25 4 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 17 Abundance Scan 2804 (30.732 min): 9676.D (-) m/ z 73.10 100.00%| 73 J
5000 147 221 281 355 429 ' i ■ ■ ' 1 i 30.40 30.60 30.80 31.00
m/z-> 45 -4 r ............ 50 ........ .1 1 1 I 1 * 1 1 1 l 1 ‘ ‘ I 1 > 100 150 200 250 300 X 350 400 ..8.89177 .......... 450 500 550 m/z 147.05 29.25% Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73
147 .................................... ........... 5000 267 355 30.40 30,60 30.80 31.00 429 45 207 m/z 221.10 17.33%
miz-> 50 100 150 200 250 300 350 -400 450 500 550 Abundance #39584: Silanamine, N-[2,6-dimethyl-4-[(trimethylsilyl)oxy] 73 281 ............................................. 209 30.40 30.60 30,80 31.00 5000 m/z 355.10 13.81% 45 251 179 120 147 ■ ' I ' ' ' ' I 111 ■ 1 ' — 1 '1 । 1 1 1 1 i ' ■ ■ 1 । 1 1 1 ' i 1 1 1 1 । 1 1 1 1 1 1 1 miz-> 50 100 150 200 250 300 350 4(X) 450 500 550 Abundance #60503:3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73 30.40 30.60 30.80 31.00 rn/z 281.00 12.36%| 5000 147
221 281 ■ • i ■ ■ ■ ■ i • • > ■ i ■ > > i j । 327 415 519 561 ' 4+1) ' 1 ' i 1 1 ' ' i ■ 1 ' ' i ‘ '■ ■ ' i 1 ' 1 1 i ' I mz—> 50 100 150 200 250 300 350 400 450 500 550 30.40 30.60 30.80 31.00
9676.D GCMS0520.M Tue May 21 11:39:24 2002 Page 13
NYC-WTC_000023808
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NYC-WTC_000023649
Laboratory report showing GC/MS blank analysis for sample AE09676 with non-detect results for volatile organic compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039588
Laboratory report documenting GCMS analysis of sample AE06455 conducted on April 19, 2002, by the DEP.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005394
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02604.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009835
Calibration data for GCMS analysis using 625/TCLP method with deuterated compound reference standards recorded on February 21, 2002.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038871
Laboratory report documenting GCMS analysis of sample AE02575 conducted on March 25, 2002, identifying other unknown compounds.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039497
Laboratory report documenting GCMS analysis of sample AE06449 conducted on April 19, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005415
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02645.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039469
Laboratory report documenting GCMS analysis of sample AE06430 conducted on April 19, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005367
Laboratory report showing non-detectable results for nitrosamines and chlorinated solvents in GCMS blank.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047979
GCMS analysis report for sample AE05749 showing surrogate recovery and unknown compounds from April 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013943
TCLP calibration table document dated May 24, 2002, listing deuterated standards and response factors for GCMS analysis.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039611
Laboratory report documenting GCMS analysis of sample AE06456 conducted on April 19, 2002, by the DEP.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000023646
Department of Environmental Protection administrative record sheet for World Trade Center site activities dated May 2002.
Filed in the same folder
NYC-WTC_000023647
Technical data file header page from a GCMS analysis run associated with the World Trade Center site in May 2002.
Filed in the same folder
NYC-WTC_000023649
Laboratory report showing GC/MS blank analysis for sample AE09676 with non-detect results for volatile organic compounds.
Filed in the same folder
NYC-WTC_000023662
Laboratory report showing GC/MS calibration data for volatile organic compounds analyzed on May 20-21, 2002.
Filed in the same folder
NYC-WTC_000023666
Laboratory report showing GC/MS reference analysis for sample AE09676 with quantitative results for volatile organic compounds.
Filed in the same folder