GCMS analysis results for sample AE06430, April 2002

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\APR1702\6430.D Vial: 6 Acq On : 17 Apr 2002 1:08 pm Operator: Sample : gc/ms scan 3/19 fb Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 16 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T. 34.90 0.79 ug/1 92473 Chrysene-dl2 33.64 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 l,l,l,5,7,7,7-H4ptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 25 2 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 25 3 1 -Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 23 4 Trisiloxane, 1/1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 16 Abundance Scan 3252 (34.896 min): 6430.D (-) m/ z 72.95 100.00% 73

147 5000 221 281 355 1 - । 1 • TIE 429 34.60 34.80 35.00 35.20 44i ’ ‘ | r ■ i ' TT ■ ■ , 191, , ' 1 1 i" ' -1 1 ‘I ' 11 1 I 11327, 401 r ' i TT 11/tLk.L p-ri i । n- m/z 147.00 57.65% mz—> 50 100 150 200 250 300 350 400 450 500 550 Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73 __ 147 / 5000 267 11 355 34.60 34.80 35.00 35.20 429 207 m/z 221.05 43.16% 45

' ’I TT ' ' i ■ ' ' 1 i 1 1 1 1 i 1 ' ' 1 i 1 ' 1 1 i ■ ■ 1 ' i 1 1 1 1 i 1 ■ 1 ■ i ■ ■ 1 ■ i r 1 ■ 1 i ' ■ rn/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-Isopropoxy-1 ,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73 -- 34.60 34.80 35.00 35.20 5000 m/z 281.05 28.03% 147 221 281 327 I 415 519 561 'D.U.H711.117/1.I.11.111/1/*/1/11/L.T ‘1 । 1 1 ■ ' i 1 ' 1 T i. ’ 1 ■ ' .i ' 1 ' * 113 T I ' 1 ti/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether 73 34.60 34.80 35.00 35.20 m/z 355.05 27.18%| 207 5000 147 34 103 281 — ' ' l 1 ' miz—> 50 100 150 200 250 300 350 400 450 500 550 34.60 34.80 35.00 35.20

6430.D GCMS0412.M Thu Apr 18 09:09:32 2002 Page 16

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