GCMS analysis results for sample AE06430, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\APRI702\6430.D Vial: 6 Acq On : 17 Apr 2002 1:08 pm Operator: Sample : gc/ms scan 3/19 fb Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 15 3-Isopropoxy-l, 1,1,7,7,7-hexam Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

32.24 0.96 ug/1 111833 Chrysene-dl2 33.64

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Isopropoxy- 1,1, 1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 37 2 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 25 3 Silanamine, N-[2,6-dimethyl-4-[(tri 281 C14H27NOSi2 072088-09-6 22 4 Trisiloxane, 1,4,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 16 Abundance Scan 2963 (32.243 min): 6430.D (-) m/ z 73.00 100.00% 73

5000 147 221 281 ।- - — i p i s r pi — i — — 355 429 32.00 32.20 32.40 32.60 45 117 , 1911 . 249 1, 325, 1 . ' TIT 1 ■ 1 i ■ 1 1r 1 i ' ' ' ; I ' "' 1 1 11 TI . ."i r | . I i r |li 401 1 1 I I I I I ] J I J J I I T m/z 147.00 43.95% ti/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-Isopropoxy-1 ,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73

5000 1 1 i 1 ■ 1 i ■ • 147 32.00 32.20 32.40 32.60 m/z 221.05 31.70% 221 21 327 415 519 561 ‘11l.—1")1111111/1/111/1/*/*/1/1/1//11/1/1//11/1T ■ ■ i ' ■ ■ ■ i ■ ■ ■ ■ i ■ ■ i ■ ■ m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether Th

' ' I ' ' 1 1 1 1 1 1 ' 1 1 1 32.00 32.20 32.40 32.60 207 5000 147 m/z 280.95 22.36% 34 103 281

mz->50 1 1 ' I ' 1 ' ' I ' 100 LL 150 200 250 300 350 400 395 450 500 482 550 Abundance #39584: Silanamine, N-[2,6-dimethyl-4-[(trimethylsilyl)oxy] 1 1 4 ,44 A I AAA- 1 , 4 73 32.00 32.20 32.40 32.60 281 m/z 355.05 19.27% 209 5000 45 251 179 120147 I .................... ----- —7)111"1111/1/111/1/1/—1/11//1/1//1/11/13 ■ ' ' I ■ ' ■ ' 1 1 1 m/z—> 50 100 150 200 250 300 350 400 450 500 550 32.00 32.20 32.40 32.60

6430.D GCMS0412.M Thu Apr 18 09:09:31 2002 Page 15

NYC-WTC_000039490