NYC-WTC_000039588
Laboratory report documenting GCMS analysis of sample AE06455 conducted on April 19, 2002, by the DEP.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Document / 20 pages
GCMS analysis results for sample AE02575, March 2002
Machine-extracted title · confidence 90%Laboratory report documenting GCMS analysis of sample AE02575 conducted on March 25, 2002, identifying other unknown compounds.
NYC-WTC_000038871–000038890Folder label: “GCMS X 3/4/02 A 3/20/02”
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NYC 9/11 Public Portal Document Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\MAR1902\2575.D Vial: 24 Acq On : 21 Mar 2002 3:41 am Operator: Sample : gc/ms scan 3/4 Inst : GC/MS 209 Mise : Multiplr: 1.0 0 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 10 1,1,1,5,7,7,7-Heptamethyl-3,3 - Concentration Rank 8
R.T. EstConc Area Relative to ISTD R.T.
3 0.85 0.36 ug/1 55402 Chrysene-dl2 33.72
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 l,l,l,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 38 2 3-Isopropoxy-1,171,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 37 3 3-Trimethylsilyloxystearic acid, tr 444 C24H5203Si2 000000-00-0 23 7... i.... ' N- ..[2,Scan6-dimethyl-4- 4 Silanamine, Abundance (-) 281 C14H27NOSi2 2810 (30.845 min): 2575.D[ (tri m/ z 072088-09-6 73.0.0 100.00% 14 73
5000- 147 221 281 355 -A-- 429 30.60 30.80 31.00 31.20
m/z--> 45 50 117 • i r 4— r +12144 • 327, 4 i ■ ■ ' ■ i ■ ■ ' * i • 1 — 401 [ — 400 —— —— 450 500 550 m/z 147.00 42.69% 100 150 200 250 300 350 Abundance #56714: 1,1,i,5,7.7.7-Heptamethyi-3,3-bis(trimethyisiioxyjt 73
147 --........... 5000 267 355 429 30.60 30.80 31.00 31.20 45 207 m/z 221.0,5 30.75% .............. —............... — 1 1 i ‘ 1 m/z->__ 50 100 150 200 250 300 350 400 450 500 550 Abundance 73 1’1/1/1/1/11.1 ’ 1 | 1
30.60 30.80 31.00 31.20 5000 m/z 355.05 25.56% 147
221 281 327 415 519 561 1 1 i ' ' 1 1 i 1 ' ■ ■ i ' 1 1 ■ i 1 ' m/z-> 50100150 200 250 300 350 400 450 500 550 Abundance #56734: 3-Trimethylsilyloxystearic acid, trimethylsilyl est ' ' I r ' ' ‘ I ' 1 1 1 1 1 ' 1 1 1 1 ' 73 30.60 30.80 31.00 31.20 m/z 281.10 17.86% 5000 147 233
313 429 189 339 387 _ — m/z-> 50 100 150 200 250 30G 350 400 450 500 550 | 30.60 30.80 31.00 31.20
2575.D GCMS0308.M Thu Mar 21 14:24:03 2002 Page 10
NYC-WTC_000038887
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