Laboratory report documenting GCMS analysis of sample AE06449 conducted on April 19, 2002.
NYC-WTC_000039497–000039521Folder label: “GCMS X 3/19/02 A 4/17/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\l\DATA\APR1702\6449.D Vial: 7 Acq On : 17 Apr 2002 2:06 pm Operator: Sample : gc/ms scan 3/19 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 13 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 32.24 0.65 ug/1 74021 Chrysene-dl2 33.65 Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 1,1,1,5,7,7,7-Heptamethyl-3,3-bis (t 444 C13H40O5Si6 038147-00-1 32 2 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 25 3 3-Isopropoxy-1,1,1,7, 7,7-hexamethyl 576 C18H5207Si7 071579-69-6 16 4 3-Isopropoxy-1,1,1,3,5,5-hexamethyl 354 Cl2H34O4Si4 072182-11-7 10 Abundance Scan 2962 (32.240 min): 6449.D (-) m/ z 73.00 100.00% 73
5000 147 221 281 355 429 32.00 32.20 32.40 32.60 , 325 | TITImmum 1911 40 401 1............. m/z 147.00 ■ ' 1 ' ■ 1 1 ' 11'1 ' ' 1 1 1 ' 1 ‘ 1 ' 1 1 ' 1 1 1 ' 1 1 ' ' 44.21%| miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73
147 5000 267 TIN 14 ' 355 429 32.00 32.20 32.40 32.60 45 207 m/z 221.05 31.83% | I 1 ■ ' ' ' 1 ‘ 1 1 1 ■ 1 1 1 । 1 < > 1 [ 1 1 mfz~> 50 100 150 200 250 300 350 400 450 500 550 Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147 1 ■ i ' ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ 281 32.00 32.20 32.40 32.60 5000 m/z 281.00 23.66%l
369 207 249 | 338 L —H ------------ — , , —L I, , , m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503:3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim _ AAAL wy AA , , AMA 73 32.00 3220 32'40 32.60 m/z 355.05 19.61% 5000 147
221 281 327 1 415 519 561 ' ' i ' ' ' 1 1 ' ' ■ ■ 1 ■ 1 1 ■ i ■ ■ ■ 1 r1 "i'll' 1/17/11T11/11111-7111/3.T m/z—> 50 100 150 200 250 300 350 400 450 500 550 32.00 32.20 32.40 32.60
6449.D GCMS0412.M Thu Apr 18 09:10:56 2002 Page 13
NYC-WTC_000039516
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NYC-WTC_000039469
Laboratory report documenting GCMS analysis of sample AE06430 conducted on April 19, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039588
Laboratory report documenting GCMS analysis of sample AE06455 conducted on April 19, 2002, by the DEP.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038871
Laboratory report documenting GCMS analysis of sample AE02575 conducted on March 25, 2002, identifying other unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039611
Laboratory report documenting GCMS analysis of sample AE06456 conducted on April 19, 2002, by the DEP.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039453
Laboratory report documenting GCMS blank analysis of sample AE06430 conducted on April 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039545
Laboratory report documenting GCMS analysis of sample AE06452 conducted on April 19, 2002, by the DEP.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005415
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02645.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005394
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02604.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023789
Instrument log and analysis summary for GCMS testing of sample AE09676 conducted on May 23, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000060478
DEP laboratory report of GCMS analysis for sample AE06635 conducted on April 18, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009835
Calibration data for GCMS analysis using 625/TCLP method with deuterated compound reference standards recorded on February 21, 2002.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047979
GCMS analysis report for sample AE05749 showing surrogate recovery and unknown compounds from April 2002.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000039437
Department of Environmental Protection site log sheet for the World Trade Center area covering March and April 2002.
Filed in the same folder
NYC-WTC_000039438
Fragmented page from a GCMS record series dated April 2002 within DEP Box 23 archives.
Filed in the same folder
NYC-WTC_000039441
Calibration report for GCMS analysis of sample AE06430 conducted on April 17, 2002.
Filed in the same folder
NYC-WTC_000039445
Laboratory report documenting GCMS reference analysis of sample AE06430 conducted on April 17, 2002.
Filed in the same folder
NYC-WTC_000039453
Laboratory report documenting GCMS blank analysis of sample AE06430 conducted on April 17, 2002.
Filed in the same folder