GCMS analysis results for sample AE06450, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\APR1702\6450.D Vial: 8 Acq On : 17 Apr 2002 3:05 pm Operator: Sample : gc/ms scan 3/19 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 3 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T.

37.31 0.49 ug/1 36845 Perylene-d12 37.87 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 l,l,l,5,7,7,7-Hdptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 25 2 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 23 3 3-Isopropoxy-11, 1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 17 43-Trimethylsilyloxystearicacid,tr444C24H5203Si2 000000-00-0 10 Abundance Scan 3514 (37.308 min): 6450.D (-) m/z 73.00 100.00% 73

5000 147 221 355 281 429 37.00 37.20 37.40 37.60 l i 1 ■ i ■ 1 ■ ' i ■ ' ■ ■ i 1 ■ 191 252_ * 1 1 11 1 1 1 ' ' | 1 ' i 1 ‘ ■ 1 । ' 1 1 1 । ' ' m/z 147.00 48.89% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsi!oxy)t 73

147 5000 267 355 37.00 37.20 37.40 37.60 429 45 207 m/z 221.05 42.51% — 1111, I -----...... 4__ 111111/1/11/1.1/1.1 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73 A1 1 i I ■ ■ ■ ■ j ■ ■

207 37.00 37.20 37.40 37.60 5000 147 m/z 355.05 28.26% 34 103 281

mz-> 50 100 150 .... LAL 200 250 300 350 400 450 T,. 500 482 550 Abundance 73 #60503: 3-lsopropoxy-1,1,1,7,7,7-hexarnethyl-3,5,5-tris(trim 37.00 37.20 37.40 37.60 A ‘ 1 * 1 1

m/z 281.00 21.57% 5000 147

221 281 327 _.......... L I 415 519 561 non ' ' i ' ■ ' 1 i ' 1 ' ' i ' ' i ' ' 17-1/1/1/11/1.1 m/z—> 50 100 150 200 250 300 350 400 450 500 550 37.00 37.20 37.40 37.60

6450.D GCMS0412.M Thu Apr 18 09:11:36 2002 Page 3

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