Laboratory report documenting GCMS analysis of sample AE06430 conducted on April 19, 2002.
NYC-WTC_000039469–000039496Folder label: “GCMS X 3/19/02 A 4/17/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\APR1702\6430.D Vial: 6 Acq On : 17 Apr 2002 1:08 pm Operator: Sample : gc/ms scan 3/19 fb Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 17 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 36.09 0.98 ug/1 80534 Perylene-dl2 37.87 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 35 2 l,lzl,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 23 3 3-Trimethylsilyloxystearic acid, tr 444 C24H5203Si2 000000-00-0 16 4 1 -Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 13 Abundance * Scan 3382 (36.090 min): 6430.D (-) m/1 z 73.00 100.00% 73
147 5000 221 281 355 429 ' ' l 1 ‘ 35.80 36.00 36.20 36.40 40 }96 117 TT " 1111 'I ’ “ U1" T 191 253 1 ih I . , 111 "I'' "I11111 325 , i J1. J, _ 11 ""I1 ETTTT " i" " i1"11' 401 _ m/z 147.00 62.47% mlz—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147 --- 5000 35.80 36.00 36.20 36.40 | 281 m/z 221.05 45.38% 45 369 117 207 249 TIT TT ।" " ।1 । i T i i । i । i i । i I T i । i I i i । i i i i । i T i i [ 11 . .. ।. TTI"TTTTT ।. 11111—0111—011 11 । < । > miz-> 40 60 80 1001201401601802002 20240260280300320340360380400420 Abundance #56714:1,1,1,5,7,7,7-Heptamethyi-3,3-bis(trimethylsiloxy)t 73 • • i 1 ' 1 • i 11 i ■
147 35.80 3600 36.20 36.40 5000 267 m/z 355.05 31.93% 355 429 45 207 — TTTTTTT ....... | |.......... HrTDTTTTT I ■1 “ I miz-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #56734:3-Trimethylsilyloxystearic acid, trimethylsilyl est i * 1 * 1 I ' 1 73 35.80 36.00 36.20 36.40 m/ z 2 81.00 27.00%|
m/z—> 5000
i" " i" ‘ ■ i' “111' ■' i 147
189 233
11 11 i 11 11 i 11 11 111 'i n 111 111
40 60 80 100120140160180200220240260280300320340360380 400 420 313 I, 339 11"' I" n 11'' 11111 387 -P 429 | •J WWMMW
35.80 36.00 36.20 3640
6430.D GCMS0412.M Thu Apr 18 09:09:33 2002 Page 17
NYC-WTC_000039492
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NYC-WTC_000039497
Laboratory report documenting GCMS analysis of sample AE06449 conducted on April 19, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039588
Laboratory report documenting GCMS analysis of sample AE06455 conducted on April 19, 2002, by the DEP.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038871
Laboratory report documenting GCMS analysis of sample AE02575 conducted on March 25, 2002, identifying other unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039611
Laboratory report documenting GCMS analysis of sample AE06456 conducted on April 19, 2002, by the DEP.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039453
Laboratory report documenting GCMS blank analysis of sample AE06430 conducted on April 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005415
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02645.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005394
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02604.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023789
Instrument log and analysis summary for GCMS testing of sample AE09676 conducted on May 23, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009835
Calibration data for GCMS analysis using 625/TCLP method with deuterated compound reference standards recorded on February 21, 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000039437
Department of Environmental Protection site log sheet for the World Trade Center area covering March and April 2002.
Filed in the same folder
NYC-WTC_000039438
Fragmented page from a GCMS record series dated April 2002 within DEP Box 23 archives.
Filed in the same folder
NYC-WTC_000039441
Calibration report for GCMS analysis of sample AE06430 conducted on April 17, 2002.
Filed in the same folder
NYC-WTC_000039445
Laboratory report documenting GCMS reference analysis of sample AE06430 conducted on April 17, 2002.
Filed in the same folder
NYC-WTC_000039453
Laboratory report documenting GCMS blank analysis of sample AE06430 conducted on April 17, 2002.
Filed in the same folder