GCMS analysis results for sample AE04730, April 2002

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR26O2\473O.D Vial: 12 Acq On : 26 Mar 2002 8:36 pm Operator: Sample : gc/ms scan 3/4 Inst : GC/MS 209 Mise : Multiplr: 1,00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 3

R.T. EstConc Area. Relative to ISTD R.T.

36.14 0.68 ug/1 52805 Perylene-dl2 37.93

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Trisiloxane, Z,1,1,5,5,5-hexamethyl 384 C12H36O4Si5 003555-47-3 35 2 1-Monolinol^ylglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 25 3 l,l,l,5,7,/7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 17 4 Tris(trimsthylsilyl)borate 278 C9H27BO3Si3 004325-85-3 10 Abundance /3 Scan 3387 (36.136 min): 4736.0 (-) m/ z TsTon... ioo7oo% 147 5000 221 281 355 _35JO_36^OO_36.^_364O_____ 191 I, , m/z 147.00 61.36”^ .m/Z;-? 50 100 150 200 250 350 300 400 450 Abundance #74103: Trisiloxane, 1,1,1,5,5,5-he'xamethyl-3,3-bis[(trimet 73 147

5000 281 35.80 36.00 36.20 36.40____ 45 369 m/z 221.05 44.73%

rn/5;>____ -V 50 100 117 150 200 207 250 249 , 300 350 400 450 Abundance #5cSrl: l-Monolirioieoyigl’yce'oi tnmetliyisiiyl other 73

207 35.80 36.00 36.20 36.40_____ 5000 147 m/z 281.10 28.55% 34 103 281 r-r-r-,--r-r-7,--r-r-r-i--A^-r-rVr-r-r-r-r-r-r-r4^^

ni/z-;>. 50 100 150 200 250 300 350 400 450 Abundance - J- Ji g “ j-Heptamethyi-S.3-bis(trimethyisiioxy )t 713 35.80 36.00 36.20 36.40 m/z 355.05 22.17% 147 5000 267 355 429 45 207 I I II \\ rr)/z--> 50 100 150 200 250 300 350 400 450 35.80 36.00 36.20 36.40

4730.D GCMS0308.M Thu Mar 28 16:31:49 2002 Page 2

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