GCMS analytical results for sample AE03827, March 29, 2002

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Data File : C:\HPCHEM\1\DATA\MAR2202\3827.D Vial: 8 Acq On : 23 Mar 2002 1:00 am Operator: Sample : gc/ms scan 2/20 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

37.39 1.16 ug/1 ' 81298 Perylene-dl2 37.97

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Trisiloxane, 1,1,1,5 ,3,5-hexamethyl 384 C12H3604Si5 003555-47-3 10 2 1,1,1,5,7,7,7-Heptam/thyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 10 3 Benzoic acid, 2,4-bis [(trimethylsil 370 C16H30O4Si3 010586-16-0 9 4 Phenethylamine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 9 Abundance Scarf 3524 (37.393 min): 3827.D (-) m/ z 73.0,0' 100.00% 73

147 5000 - 221 281 355 193 I . 253 429 37.00 37.20 37.40 37.60 37.80 44 .96 TTgruta ’r —#... —mm .......... —..... . ■| L ' I' n ‘I' m/ z 147.00 60.13% m/z-> 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380 400420 Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147 281 5000 a—-4A--AAAA-A—4=44 37.00 37.20 37.40 37.60 37.80 369 m/z 221.05 43.73% 207 I | • " 1 r " »11 "• | n H | < 1111 I i ■ ’ ■' i 249 . 338 । TTTTTTTTTTTTTTTTTTTTT " ■ I ’"' i'"' i r"■i T m/z-> 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance #56714: 1.1.1.5,7.7.7-Heptamethyl-3.3-bis(trimethylsilexy)t 73

147 37.00 37.20 37.40 37.60 37.80 5000- 267 m/z 281.0,5 25.97% 355 429 45 207 T’EEIIEEEITTEEIETTTFTTTTT 1 ‘ ‘I I" 1111 ‘" 11"11 r"■i 11" 11' m/z-> __ 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380400420 Abundance #73975: Benzoic acid, 2,4-bis[(trimethylsilyl)oxy]-, trimet 73 37.00 37.20 37.40 37.60 37.80 m/z 355.05 23.03% 5000 355 45 133 ! 193 , 223 . 281 I T’T’TT i ■" ■ f i'", i,,,,, P1 "i TWggg r 1 1 ' ' 1 I1 - I ♦ *1■ ■ । ■ ■ ■ ■ । ' 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 37.00 37.20 37.40 37.60 37.80

3827.D GCMS0308.M Tue Mar 26 14:56:10 2002 Page 2

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