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GCMS analytical results for sample AE03827, March 29, 2002

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Laboratory report listing detection results for volatile organic compounds in sample AE03827 analyzed on March 29, 2002.

NYC-WTC_000038042–000038053

Folder label: “GCMS X 2/20/02 A 3/22/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR2202\3827.D vial: 8 Acq On 23 Mar 2002 1:00 am Operator: Sample : gc/ms scan 2/20 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 1-Monolinoleoylglycerol trimet Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

36.15 0.51 ug/1 35751 Perylene-dl2 37.97

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Monolinoleoylg cerol trimethylsi 498 C27H54O4Si2 054284-45-6 23 2 3-(3-Hydroxyphe 1)-3-hydroxypropio 398 C18H3404Si3 000000-00-0 13 3 Dithioerythrit , tetrakis(trimethy 442 C16H42O2S2S14 000000-00-0 12 4 2-Methoxyphenylpyruvic acid, di-TMS 338 C16H2604Si2 000000-00-0 10 Abundance / Scan 3389 (36.154 min): 3827.D (-) m/z 72.95 100.00% 73

147 5000 221 281 355 TT ■ i ' ' ' ■ i ' 429 1 49 1211 , 1 1, 32741 — 35.80 36.00 m/z 147.00 36.20 36.40 56.94% im/z-> 50 100 150 200 250 300 350 400 450 Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73

207 5000 - 147 PA—4A—4 35.80 36.00 36.20 36.40 34 103 i 281 m/z 221.05 '39.53% 1 i 395 482 m/z-> 50 100 150 200 250 300 350 400 450 Abundance #53668: 3-(3-Hydroxyphenyl)-3-hydroxypropionic acid, tri-TMS 73 267 "" 35.80 36.00 36.20 36.40 5000 147

207 398 47 , 293 341 . AAA- VWMwAA m/z-> 50 100 150 200 250 300 350 400 450 Abundance #56591: Dithioerythritol, tetrakis(trimethylsilyl)- ‘ii I’T 73‘ 35.80 36.00 36.20 36.40 m/z 355.05 19.78% 5000 221 45 147 | 1101 —173 11 I247 36404 m/z-> 50 100 150 200 250 300 350 400 450 35.80 36.00 36.20 36.40

3827.D GCMS0308.M Tue Mar 26 14:56:05 2002 Page 1

NYC-WTC_000038049

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NYC-WTC_000038049Source: NYC Law Department, mirrored locally

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