GCMS analysis results for sample AE04844, April 2002

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Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\M7lR2802\4844.D Vial: 23 Acq On : 29 Mar 2002 6:21 am Operator: Sample : gc/ms scan 3/5 Inst : GC/MS 209 Mise • : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 1-Monolinoleoylglycerol trimet Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

36.14 0.66 ug/1 32133 Perylene-dl2 37.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual 11-Monolinoleoylgly/erol trimethylsi 498 C27H54O4Si2 054284-45-6 33 23-Isopropoxy-1,1,7, 7,7,7-hexamethyl 576 C18H52O7Si7 071579-69-6 12 31,1,1,5,7,7,7-Hebtamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 10 4Trisiloxane, 1,1(, 1,5,5,5-hexamethyl 384 C12H36O4Si5 003555-47-3 9' Abundance Scan 3387 (36.139 min): 4844.D (-) m/ z ■7'2795.■.iqq7oq% 7|3

147 , 5000 221 281 355 49 429 . _318Q_ 36^J6.2jO_J6.46_____ --h .......... ’m/z’ 147 . on" 52.66% 50 100 150 200 250 300 350 400 450 500 550 Abundance #58871: 1-Monoiinoieoyiglycerol trimethylsilyl ether 73

207 5000 147 I 35.80 36.00 36.20 36.40 34 103 281 m/z 221.0.5 32.70%. I :i 395 482 m/^^___ 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-l£Opi-cBoxv-i .1.1.(.r.r-hoxamett'.vl-a.S.S-irisctnm 73

I 35.80 36.00 36.20 36.40_____ 5000 m/z 281.10 23.03% 147

221 281 227 415 '.......... j..... ) ....... .......... 519 561 {n/^>........ 50 100 150 200 250 300 350 400 450 500 550 'Abundance #56714: 1,1,1,5,7.7,7-Heptamethyi-3,3-bis(trimethyisiioxy)t 7l3 35.80 36.00 36.20 36.40 m/z 355.05 22.46% 147 5000 267

u 355 429 207

I fn/2--> 50 100 150 200 250 300 350 400 • 450 500 550 35.80 36.00 36.20 36.40

4844.D GCMS0308.M Mon Apr 01 15:51:25 2002 ,Page 1

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