GCMS analysis results for sample AE04844, April 2002

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Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR2802\4844.D Vial: 23 Acq On : 29 Mar 2002 6:21 am Operator: Sample : gc/ms scan 3/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

37.37 0.74 ug/1 35592 Perylene-dl2 37.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Trisiloxane, y, 1,1,5,5,5-hexamethyl 384 C12H36O4Si5 003555-47-3 12 2 N-Methyladrenaline, tri-TMS 413 C19H39NO3Si3 000000-00-0 10 3 1,2-Benzened'icarboxylic acid, bis(t 310 C14H22O4Si2 002078-22-0 9 4 3-Isopropo^-l, 1,1,7,7,7-hexamethyl 576 C18H52O7Si7 071579-69-6 9 Abundance Scan 3521 (37.369 min): 4844.D (-) ........ m/z.... 73?^.... foo;oo% 713

147 5000 221 2?^ 355

m/z-> 40 rvtrrrrV X* J.,,.. u. 40 60 80 100120140160 180 200 220 240 260 280 300 320 340 360 380 400 420 429 37.00 37,20 37.40 37,60 m/z 147.00 63.62% Abundance #52459: T risiloxane, 1,1,1,5,5,5-hexameihyl-3,3-bis[’(trimet 1 •7 1 281 i i 5000 37,00 37,20 37,40 37,60 369 m/z 221.05 47.05% 207 249, I 338 ( yrrTTyTTTTyTTSTyi^TT^ m/z-> 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380 400420 Abundance #54808: N-Methyladrenaline, tri-TMS 73

37.00 37.20 37,40 37,60 5000 355 m/z 281.05 29.90% 45 207 267 323 I 'm/2->.... 4o' 60 80 'l6o 120 140 160 'l80 200 220 240 260 280 300 320 340 360 380 400 420^ ■Abundance #72972: i ,2-Benzenedicarboxylic acid, bis(trimethylsiryl) e 1 7 37.00 37.20 37.40 37.60 73 m/z 355.OS 24.39% 5000

45 295 .. I 193 221 .... ....................... ........... I" " I" I" " I m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 37.00 37.20 37.40 37.60

4844.D GCMS0308.M Mon Apr 01 15:51:29 2002 Page 2

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