GCMS analytical results for sample AE03824, March 29, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR2202\3824.D Vial: 15 Acq On : 23 Mar 2002 7 :52 am Operator: Sample : gc/ms scan 2/20 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L

Peak Number 2 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

38.84 0.83 ug/1 56776 Perylene-dl2 37.96

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Trisiloxane,/1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 27 2 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 23 3 1,2-Benzenedicarboxylic acid, bis(t 310 C14H2204Si2 002078-22-0 9 4 2(3H)-Th/azolimine, 3 -hydroxy-4 -(3 - 273 C9H8C1N3O3S 058275-70-0 9 Abundance Scan 3682 (38.844 min): 3824.D (-) m/ Z 73.00 100.00% 73

147 5000 221 281 355 191 । 429

miz-? ■ 44 i ■ ■ ■ ■ i > 50 100 150 ■l _ ■

200 ■ •

250 r p

300 ' ■

350 253, i

400 ■ ■

450 22711 500 — 550 m/z _/ 38.60 38.80 39.00 147.0062.54% 39.20

Abundance #52459: Trisiloxane, 1,1,1,5.5,5-hexamethyl-3,3-bis[(trimet 73 147 281 5000 38.60 38.80 39.00 39.20 1

. 369 47.03% । I—r mPI I -1 207r r 249 338 । 1 ' i m/z--> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-Isopropoxy-1 .1.1 l.i .7-hexamethyl-3,5,5-trs(trim 73 TGEEEEEIT । 38.60 38.80 39.00 39.20 5000 m/z 281.05 30.84% 147

221 281 327 415 519 561 ■ • i • ■ • ■ i ■ VAhN— WAw m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance * #72972: 1,2-Benzenedicarboxylic acid, bis(trimethylsilyl) e ■ ■ । ■ > • > । 147 38.60 38.80 39.00 39.20 m/z 355.05 25.94% 73 5000

45 295 1 , I, , 1 119— , 193221 .. |....... 1 1 I ' ' ■ > i • • miz-> 50 100 150 200 250 300 350 400 450 500 550 38.60 38.80 39.00 39.20

3824.D GCMS0308.M Tue Mar 26 14:53:44 2002 Page 2

NYC-WTC_000038030