TCLP calibration table review document, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\APR17O2\82O9 .D Vial: 20 Acq On : 18 Apr 2002 2:46 am Operator: Sample : gc/ms scan 4/8 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 5 l-Monolinoleoylglycerol trimet Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 44.35 0.59 ug/1 97734 Perylene-dl2 37.88 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 28 2 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 16 3 3,6-Dioxa-2,4,5,7-tetrasilaoctane , 294 C10H3002Si4 004342-25-0 16 4 2,6-Dimethyl-3,4-Xis(trimethylsilyl 311 C15H29NO2Si2 000000-00-0 14 Abundance Scan 4281 (44.349 min): 8209.D (-) m/z 147.00 100.00% 73 147 221

281 355 5000

429 ' 1 1 1 1 1 ' i ' ' 1 ' I 1 1 1 1 I ' 192 3271 44.00 44.20 44.40 44.60 H I I l i 253 | . Il ll , — ' 1 1 1 T 1 1 1 1 m/Z 221.05 92.88% I 1*11 * ‘ 1* 1 1 । ‘ 1 i ■ r ' ‘ i ' 1 1 1 1 m/z-> 50 100 150 200 250 300 350 400 450 Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73 ■ ■ / , i . । । । । j । । ।

207 5000 147 44.00 44.20 44.40 44.60 34 103 m/z 73.00 88.22% 281 482 m/z-> 50 100 150 200 250 300 350 400 450 Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147

281 44.00 44.20 44.40 44.60 5000 m/z 354.95 55.00%

369 207 249 — 338 J........ Id। m/z-> 50 100 150 200 250 300 350 400 450 Abundance #41682: 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7- * । । r । । < । । । । । l । । । । । । । । । 7 147 221 44.00 44.20 44.40 44.60 2 81.00 m/z / 50.84% 73 5000

191

m/z—> 50 J 117

100 L 150 1 ■ 'i' 200 1 250 279

300 350 400 450 ' ' I ' 1 1 ' 1 1 ' 1 1 I ' ' 1 1 I ' 1 1 1 1 1 44.00 44.20 44.40 44.60

8209.D GCMS0412.M Thu Apr 18 14:11:09 2002 Page 5

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